LAPORAN ANALISA KUALITATIF

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  • 8/19/2019 LAPORAN ANALISA KUALITATIF

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    LAPORAN PRAKTIKUM

    KIMIA KEPERAWATANPERCOBAAN I

    ANALISA KUALITATIF

    DISUSUN OLEH :

     NAMA : BELA ROMANDHA SARI

     NIM : 11 11011009

    ASISTEN :

    DOSEN PEMBINA : ROHIMATUSH SHOFIYAH, S.Si., M.Si.

    PROGRAM STUDI KEPERAWATAN

    FAKULTAS ILMU KESEHATAN

    UNIVERSITAS MUHAMMADIYAH JEMBER 

    011

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    I.2 Permasalahan

    P($'!#!+!3!% -$!)i' !+i i%i !"!+!3 :

    B!/!i'!%! $(!#i -(%/(%!+!% !)i*% ($"!#!$!% -(%/(%"!-!% "!% 8!$%!

     -($#(%&!8!!% &!%/ )($(%) B!/!i'!%! $(!#i -(%/(%!+!% !%i*% ($"!#!$!% -(%/(%"!-!% "!% 8!$%!

     -($#(%&!8!!% &!%/ )($(%)

    I.3 Tujuan

    T!% -$!)i' !+i i%i !"!+!3:

    M!'- '('-(+!!$i $(!#i -(%/(%!+!% !%i*% ($"!#!$!% -(%/(%"!-!% "!% 8!$%!

     -($#(%&!8!!% &!%/ )($(%).

    M!'- '('-(+!!$i $(!#i -(%/(%!+!% !)i*% ($"!#!$!% -(%/(%"!-!% "!% 8!$%!

     -($#(%&!8!!% &!%/ )($(%).

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    BAB II

    TINJAUAN PUSTAA

    II.1 las!"!kas! Anal!s! at!#n

    U%) !%!+i#i# !+i)!)i2 #i#)('!)i !)i*%!)i*% "i!+#i2i!#i "!+!' +i'! /*+*%/!%

     ($"!#!$!% #i2!)#i2!) !)i*% i) )($3!"!- (($!-! $(!/(%. R(!/(% /*+*%/!% &!%/ "i-!!i

    %) +!#i2i!#i !)i*% &!%/ -!+i%/ '' !"!+!3 !#!' +*$i"!, 3i"$*/(% #+2i"!, !'*%i'

    #+2i"! "!% !'*%i' !$*%!). K+!+i#2i!#i i%i "i"!#!$!% !)!# !-!!3 #!) !)i*% ($(!#i

    "(%/!% $(!/(%$(!/(% i%i "(%/!% '('(%) (%"!-!% !)! )i"!.

    M(%$) G. S;(3+! 619. G*+*%/!% III, !)i*% /*+*%/!% i%i )! ($(!#i "(%/!% !#!' +*$i"! (%5($, !)!-%

    "(%/!% 3i"$*%/(% #+2i"! "!+!' #!#!%! !#!' 'i%($!+ (%5($. N!'%, !)i*% i%i

    '('(%) (%"!-!% "(%/!% !''*%i' #+2i"! "(%/!% #!#!%! %()$!+ !)! !'*%i!!+.

    K!)i*%!)i*% /*+*%/!% i%i !"!+!3 *!+)6II7, %i(+6II7, (#i6II7, (#i6III7, $*'i'6III7,

    !+'i%i', 4i%, "!% '!%/!%6II7.

    ?. G*+*%/!% IV, !)i*% /*+*%/!% i%i )! ($(!#i "(%/!% $(!/(% /*+*%/!% I, II, III. K!)i*%

    !)i*% i%i '('(%) (%"!-!% "(%/!% !''*%i' !$*%!) "(%/!% !"!%&! !''*%i'

    +*$i"!, "!+!' #!#!%! %()$!+ !)! #("ii) !#!'. K!)i*%!)i*% /*+*%/!% i%i !"!+!3

    !+#i', #)$*%)i', "!% !$i'.

    =. G*+*%/!% V, !)i*%!)i*% &!%/ '', &!%/ )i"! ($(!#i "(%/!% $(!/(%$(!/(%

    /*+*%/!% #((+'%&!, '($-!!% /*+*%/!% !)i*% &!%/ )($!3i$, &!%/ '(+i-)i i*%i*%

    '!/%(#i', %!)$i', !+i', !'*%i', +i)i', "!% 3i"$*/(%.

  • 8/19/2019 LAPORAN ANALISA KUALITATIF

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    II.2 las!"!kas! Anal!s!s An!#n

    A%i*% '($-!!% i*% &!%/ '!)!% )*)!+%&! %(/!)i2 !i!) !"!%&! (%!i!% '+!3

    (+()$*%. Mi#!+%&! : !)*' +*$i% 6C+7 "!-!) '('-($*+(3 )!'!3!% #!) (+()$*% %) 

    '(%"!-!) i*% +*$i"! 6C+7. N!)$i' +*$i"! 6N!C+7, &!%/ "i(%!+ #(!/!i /!$!' "!-$,

    "i#() #(%&!8! i*%i 6i*%i 5*'-*%"7 !$(%! "i(%) "!$i !)i*% "!% !%i*%. A)*' "!-!)

    (3i+!%/!% !)! '('-($*+(3 +(i3 "!$i #!) (+()$*%. C*%)*3 i*%i*% &!%/ )($(%) "(%/!%

    (3i+!%/!% !)! '('-($*+(3 +(i3 "!$i #!) (+()$*% !"!+!3 M/ @, F(>@, S, "!% N>, N!@ "!%

    C+ I*%i*% i%i "i#() i*% '*%*!)*'i !$(%! i*%i*% i%i '(%/!%"%/ 3!%&! #!) !)*'.

    P(%/i!% !%i*% "i+!!% #()(+!3 i !)i*%. P(%/i!% )($3!"!- !%i*% $(+!)i2 +(i3 #("($3!%!

    !$(%! /!%//!%/!%//!% "!$i i*%i*% +!i% &!%/ !"! "!+!' +!$)!% 'i%i'!+ 6"!-!)

    "i!!i!%7. P!"! ''%&! !%i*%!%i*% "!-!) "i/*+*%/!% #(!/!i ($i) :

    1. G*+*%/!% #+2!): SO?, SO>

    , PO?>, C$ O?

    , BO>> , C$ O?

    , A#O?>,A#O>

    >. A%i*%!%i*%

    i%i '(%/(%"!- "(%/!% B!@ "!+!' #!#!%! !#!.

    . G*+*%/!% 3!+i"! : C+, B$ , I, S A%i*% /*+*%/!% i%i '(%/(%"!- "(%/!% A/@ "!+!' +!$)!%

    !#!' 6HNO>7. G*+*%/!% %i)$!) : NO>, NO

    ,CH>O. S('! /!$!' "!$i /*+*%/!% i%i

    +!$). NO>, NO

    , CH>OO .

    M(%$) G. S;(3+! 619

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    "i)i'!%/ #(!/!i A/C+ !)! % "i(%"!-!% #(!/!i %6NH?7PO?HO, #(+!%)%&! "i!!$ 

    "!% "i)i'!%/ #(!/!i %PO. A#-( &!%/ -(%)i%/ "!% -($+ "i-($3!)i!% -!"! '()*"(

    )($#() !"!+!3 (%"!-!%%&! (%"!-!%%&! '('-i%&!i (+!$)!% &!%/ (5i+ #(!+i "!% "!-!)

    "i-i#!3!% #(5!$! 2i+)$!#i. Si2!) 2i#i (%"!-!% #("('ii!% $-!, #(3i%//! '"!3 "i-i#!3!%

    "!$i +!$)!%%&! "(%/!% 2i+)$!#i, "!-!) "i55i %) '(%/3i+!%/!% -(%/*)*$, $!%

     -!$)i(+%&! 5- (#!$ #($)! (%"!-!% "!-!) "i!3 '(%!"i 4!) '$%i "(%/!% *'-*#i#i

    i'i! )($)(%).

    II.' $et#%e (arna &ersen)a(aan

    B!%&! i*%i*% )($+!$) &!%/ i)! )('i "i #(i)!$ i)! 'i#!+%&! -!"! !i$ +!),#%/!i, +i'!3, !)! -%

    "!+!' (%) -!"!)!%%&! #(-($)i -!"! )!%!3 "!%--. U%#$ +*/!' "!+!' +!$)!%%&! !!% '('(%) i*%

     -*#i)i2 !)!!)i*%, #("!%/!% %#$ %*% +*/!' !!% '('(%) i*% %(/!)i2 !)!!%i*%. M()*"( &!%/

    "i/%!!% %) '(%(%)!% (($!"!!% !)i*% "!%!%i*% )($#() "!+!' i"!%/ i'i! "i#() !%!+i#i#

    !+i)!)i2. U%)#(%&!8! !%*$/!%i "i#() !%!+i#i# !+i)!)i2 !%*$/!%i.B!%&! -(%"(!)!% &!%/ "!-!)

    "i/%!!% %) '(+!!% !%!+i#i#!+i)!)i2. I*%i*% "!-!) "ii"(%)i2i!#i ($"!#!$!% #i2!) 2i#i! "!%

    i'i!%&!.B(($!-! '()*"( !%!+i#i# !+i)!)i2 '*"($% '(%//%!!% #i2!) 2i#i! #(-($)i8!$%!, #-()$'

    !#*$-#i, #-()$' ('i#i, !)! '("!% '!/%() %)'(%/i"(%)i2i!#i i*% -!"! )i%/!) *%#(%)$!#i &!%/

    $(%"!3.N!'% "('ii!% i)! /! "!-!) '(%//%!!% #i2!) 2i#i! "!% i'i! %)'(%/('!%/!% #!)

    '()*"( !%!+i#i# !+i)!)i2 '(%//%!!% !+!)!+!)&!%/ #("($3!%! &!%/ "i-%&!i 3!'-i$ #('! +!*$!)*$i'.

    Si2!) 2i#i!&!%/ "!-!) "i!'!)i +!%/#%/ #(-($)i 8!$%!, !, )($(%)%&! /(+('%//!# !)! -% (%"!-!%

    '($-!!% i%2*$'!#i !8!+ &!%/ ($/%! %)!%!+i#i# #(+!%)%&!. T!(+ ($i) '(%%!% (($!-! i*%

    &!%/($8!$%!.T!(+ . W!$%! (($!-! i*% "!+!' -(+!$) !i$

    Jen!s !#n *arna Jen!s !#n *arna

    2+¿

    CU ¿ Bi$

      2+¿

     Mn¿ M($!3 '"!

    3+¿

    Cr¿

    Hi!   2+¿

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     Fe¿

    K%i%/ (5*+!)!%   −¿ MnO

    4

    ¿U%/

  • 8/19/2019 LAPORAN ANALISA KUALITATIF

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    B(($!-! +*/!' '('-%&!i 8!$%! %&!+! &!%/ #-(#i2i #(3i%//! "!-!)"i+!!% #(!/!i #!+!3 #!) 5!$!

    %) i"(%)i2i!#i !)i*% )($#() 6T!(+>7.T!(+ >. W!$%! %&!+! (($!-! +*/!'

    L#gam *arna L#gam *arna

     N! K%i%/ B! Hi! (%i%/!%

    K U%/ C! M($!3 (%i%/!%

    Li M($!3 S$ M($!3 )!

    BAB III

  • 8/19/2019 LAPORAN ANALISA KUALITATIF

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    $ET+D+L+,I

    III.1 Alat %an Bahan

    III.1.1 Alat

    A+!) &!%/ "i/%!!% "!+!' -$!)i% !%!+i#! !+i)!)i2 !%i*% "!% !)i*% !%)!$! +!i%,

    )!%/ $(!#i,$! )!%/ $(!#i,-(%(-i) )!%/,-i-() )()(#,*+ -i-(),;*+' -i-(),!)!%/

     -(%/!" 

    III.1.2 Bahan

    B!3!% &!%/ "i/%!!% "!+!' -$!)i' !%!+i#! !+i)!)i2 !%i*% "!% !)i*% !%)!$!

    +!i%,CUSO

    4 , P A#()!), MgSO

    4 , HgCl

    2 , K$i#)!+ Na

    2CO

    3 , K 

    2SO

    4 ,

     Na2S

    2O

    3 , KNO

    3 , KI, N!C+, N!OH, H 

    2SO

    4 ,BaCl

    2 , HC+, FeSO

    4

    III.2 Pr#se%ur Per-#aan

    A. /eaks! Pengenalan at!#n

    D!+!' $(!#i ($i) i%i 3(%"!%&! "i-($3!)i!% 8!$%! "!% (%"!-!% &!%/

    )($(%).

    1. R(!#i -(%/(%!+!% !)i*%2+¿

     Mg¿

    L!$)!% &!%/ "i-($i#! : MgSO

    4

    L!$)!% $(!/(%) : N!OH

    . R(!#i -(%/(%!+!% !)i*%+¿

     Hg¿

    L!$)!% &!%/ "i-($i#! : H/C  I 

    2

    L!$)!% $(!/(%) : KI

    >. R(!#i -(%/(%!+!% !)i*%2+¿

     Pb¿

    L!$)!% &!%/ "i-($i#! :  PbCH 

    3COO

    L!$)!% $(!/(%) : N!C+

    ?. R(!#i -(%/(%!+!% !)i*%2+¿

    Cu¿

    L!$)!% &!%/ "i-($i#! :  CuSO

    4

    L!$)!% $(!/(%) : KI

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    B. /eaks! Pengenalan An!#n

    1. R(!#i -(%/(%!+!% !%i*%2−¿

    CO3

    ¿

    L!$)!% &!%/ "i-($i#! : $i#)!+  Na2CO3

    L!$)!% $(!/(%) : H 

    2SO

    4

    . R(!#i -(%/(%!+!% !%i*%2−¿

    SO4

    ¿

    L!$)!% &!%/ "i-($i#! :  K 

    2SO

    4

    L!$)!% $(!/(%) :  BaCl

    2  

    >. R(!#i -(%/(%!+!% !%i*%

    2−¿

    S2O3¿

    L!$)!% &!%/ "i-($i#! :  Na

    2S

    2O

    3

    L!$)!% $(!/(%) : HC+

    ?. R(!#i -(%/(%!+!% !%i*%2−¿

    SO4

    ¿

    L!$)!% &!%/ "i-($i#! :  MgSO

    4

    L!$)!% $(!/(%) :  H 2SO4

    =. R(!#i -(%/(%!+!% !%i*%−¿

     NO3

    ¿

    L!$)!% &!%/ "i-($i#! :  KNO

    3

    L!$)!% $(!/(%) :  FeSO

    4

  • 8/19/2019 LAPORAN ANALISA KUALITATIF

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    BAB I0

    ANALISA DATA DAN PE$BAHASAN

    I0.1 Anal!sa Data

    B($"!#!$!% -(%/!'!)!% &!%/ )(+!3 "i+!!%, '!! "i"!-!)!% "!)! 3!#i+ !%!+i#!

    !+i)!)i2 "!$i %#$( !)i*% "!% !%i*% #(!/!i ($i):

    A. Data Has!l Anal!s!s Unsur at!#n

    Unsure

    kat!#n

    /eagent *arna mulamula Peruahan (arna En%a&an

     MgSO4  N!OH B(%i%/ T()!- (%i%/ Ti"! !"!

    H/C  I 

    2 KI B(%i%/ K(%i%/!% Ti"! !"!

     PbCH 3C   N!C+ B(%i%/ P)i3 Ti"! !"!

    CuSO4 KI Bi$ Hi! A"!

    B. Data Has!l Anal!s!s Unsur An!#n

    Unsure

    an!#n

    /eagent *arna mulamula Peruahan (arna En%a&an

    $i#)!+

     Na2CO

    3

     H 2SO

    4 B(%i%/ T()!- (%i%/ Ti"! !"!

     K 2SO

    4  BaCl

    2 B(%i%/ P)i3 ($3 A"!

     Na2S

    2O

    3 HC+ B(%i%/ P)i3 ($3 A"!

     MgSO4

      H 2SO

    4 B(%i%/ T()!- (%i%/ Ti"! !"!

     KNO3

      FeSO4 B(%i%/ K(%i%/!% Ti"! !"!

  • 8/19/2019 LAPORAN ANALISA KUALITATIF

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    I0.2 Pemahasan

    P!"! -($5*!!% !%!+i#i# !+i)!)i2 $(!#i -(%/(%!+!% !)i*%, 5!i$!% M/SO? &!%/

    "i)!'!3 "(%/!% 5!i$!% N!OH. A8!+%&! '+ M/SO? ($8!$%! (%i%/ #()(+!3 "i)()(#i N!OH

    #(!%&! = )()(# "!% "i!", 8!$%! )($#() ($!3 8!$%! '(%!"i #("ii) ($3 "!%

    !3i$%&! '(%!"i -)i3 #($)! )i"! )i'+ (%"!-!%. C!i$!% H/C+ #(!%&! '+  &!%/

     ($8!$%! (%i%/  "i)()(#i "(%/!% = )()(# 5!i$!% KI, #()(+!3 ("! 5!i$!% )($#() "i!" 

    8!$%!%&! ($!3 '(%!"i (%i%/!% "!% )i"! )($"!-!) (%"!-!%. PCH >COO #(!%&!

    '+ "i5!'-$!% "(%/!% = )()(# N!C+, !8!+%&! PCH>COO (%i%/ #()(+!3 "i5!'-$ "(%/!%

     N!C+ ('"i!% "i!" "!% )i"! )($!"i -($!3!% 8!$%! #($)! )i"! )($"!-!) (%"!-!%.

    C!i$!% CSO? #(!%&! '+ "i5!'-$!% "(%/!% 5!i$!% KI #(!%&! = )()(# &!%/ !8!+%&!

     ($8!$%! i$ #()(+!3 "i!" '!! 8!$%!%&! ($!3 '(%!"i 3i! "!% )($"!-!) (%"!-!%.

    P!"! -($5*!!% !%!+i#i# !+i)!)i2 $(!#i -(%/(%!+!% !%i*%, N!CO>  '+ "i+!$)!%

    "(%/!% 5!i$!% HSO? #(!%&! = )()(# ('"i!% "i!" "!% 3!#i+%&! !"!+!3 )i"! '(%/!+!'i

    '(%/!+!'i -($!3!% 8!$%! "!% )()!- ($8!$%! (%i%/ #($)! )i"! )i'+ (%"!-!%. K SO?

    #(!%&! '+ "i)()(#i = )()(# B!C+   "!% -($!3!% &!%/ )($!"i !"!+!3 8!$%!%&! &!%/

    !8!+%&! ($8!$%! (%i%/ '(%!"i -)i3 ($3 "!% )i'+ (%"!-!%. C!i$!% N!SO> #(!%&! 

    '+ "i)!'!3 = )()(# HC+, !8!+%&! N! SO> ($8!$%! (%i%/ ($!3 '(%!"i -)i3 ($3

    "!% )($"!-!) (%"!-!% -!"! 5!'-!% )($#(). '+ M/SO?  "i5!'-$!% "(%/!% = )()(#

    HSO?, #()(+!3 "i$(!#i!% )i"! )($!"i -($!3!% 8!$%!%&! )()!- (%i%/ "!% )i"! )i'+

    (%"!-!%. C!i$!% KNO> #(!%&! '+ "i)!'!3 "(%/!% = )()(# F(SO? '!! -($!3!% &!%/

    )($!"i &!i) -($!3!% 8!$%! "!$i (%i%/ '(%!"i (%i%/!% "!% )i"! )($"!-!) (%"!-!%.

  • 8/19/2019 LAPORAN ANALISA KUALITATIF

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    BAB 0

    ESI$PULAN DAN SA/AN

    0.1 es!m&ulan

    172+¿

    Cu¿  "!-!) "ii"(%)i2i!#i "(%/!% KI &!%/ '('(%) (%"!-!% 3i!

    7 SO?"!-!) "ii"(%)i2i!#i "(%/!%

    BaCl2  &!%/ '('(%) (%"!-!% -)i3

    >72−¿

    S2O

    3

    ¿  "!-!) "ii"(%)i2i!#i "(%/!%  HCl &!%/ '('(%) (%"!-!% -)i3

    0.2 Saran

    17 Di3!$!-!% (-!"! -$!)i!% !/!$ (%!$(%!$ '('-($3!)i!% !-!!3 #"!3

    )($(%) (%"!-!% "(%/!% 8!$%! &!%/ #(#!i "(%/!% -$*#("$.

    7 P!"! #!!) -(%/%!!% NH?OH 3(%"!+!3 )i"! '(%5i' !%&!, "!% !/!$ 5(-!)

    '(%)- *)*+ %&! !/!$ )i"! '(%&(!$ "!+!' $!%/!%

    >7 Di3!$!-!% (-!"! -$!)i!% !/!$ '(%55i #()i!- -($!+!)!% &!%/ !!% "i/%!!%

    #(-($)i -i-() )()(#, !/!$ )i"! )($*%)!'i%!#i "(%/!% 4!)4!) !)! +!$)!% &!%/ )(+!3

    "i/%!!% #((+'%&!.

  • 8/19/2019 LAPORAN ANALISA KUALITATIF

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    DATA/ PUSTAA

    Hi"!&!)i,A%!,D$!,M.Si.00=.P()% P$!)i' D!#!$ i'i! A%!+i)i.S('!$!%/.

    I%,M.S*"i ".00?. Ki'i! A%!+i)i I. M!+!%/ : JICA

    V*/(+.19

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    ampuran menjadi putih dan tidak timbul endapan

     TABUNG 1

    2 ml MgSO4 (bening) Ditamba!an " tete# NaO$

    Campuran diadu!

    Amati perubaan %arna & endapan 'ang terbentu!

     TABUNG 2

    2 ml $gCl2 (bening) Ditamba!an " tete#

    Campuran diadu!

    Amati perubaan %arna & endapan 'ang terbentu!

    ampuran menjadi keuningan dan tidak timbul endapan

    SE$A

    A. /eaks! Pengenalan at!#n

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     TABUNG *

    2 ml +bC$*COO (bening) Ditamba!an " tete# NaCl

    Campuran diadu!Amati perubaan %arna &endapan 'ang terbentu!

    ,ampuran tetap bening- tidak ada endapan

     TABUNG 4

    2 ml CuSO4 (biru) Ditamba!an " tete#

    Campuran diadu!

    Amati perubaan %arna & endapan 'ang terbentu!

    ,ampuran menjadi hijau- ada endapan

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     TABUNG 1

    2 ml Na2CO* (bening)Ditamba!an " tete# $2SO4

    Campuran diadu!

    Amati perubaan %arna & endapan 'ang terbentu!

    ,ampuran tetap bening- tidak  ada endapan

     TABUNG 2

    2 ml 2SO4 (bening) Ditamba!an " tete# BaCl2

    Campuran diadu!

    Amati perubaan %arna & endapan 'ang terbentu!

    ,ampuran menjadi putih keruh- ada endapan

    B. /eaks! Pengenalan An!#n

  • 8/19/2019 LAPORAN ANALISA KUALITATIF

    17/18

     TABUNG*

    2 ml Na2S2O* (bening) Ditamba!an " tete# $Cl

    Campuran diadu!Amati perubaan %arna & endapan 'ang terbentu!

    ,ampuran menjadi putih keruh- ada endapan

     TABUNG 4

    2 ml MgSO4 (bening) Ditamba!an " tete# $2SO4

    Campuran diadu!

    Amati perubaan %arna & endapan 'ang terbentu!

    ,ampuran tetap bening- tidak  ada endapan

  • 8/19/2019 LAPORAN ANALISA KUALITATIF

    18/18

     TABUNG "

    2 ml NO* (bening) Ditamba!an " tete# .eSO4

    Campuran diadu!

    Amati perubaan %arna & endapan 'ang terbentu!

    ampuran menjadi kekuningan- tidak ada endapan