Panduan Perkhidmatan Makmal Makanan-edit · dikeluarkan adalah diterima sepenuhnya. < v v P v u l u...
Transcript of Panduan Perkhidmatan Makmal Makanan-edit · dikeluarkan adalah diterima sepenuhnya. < v v P v u l u...
PANDUAN PERKHIDMATAN MAKMAL MAKANAN
KEMENTERIAN KESIHATAN MALAYSIA
Oleh
KEMENTERIAN KESIHATAN MALAYSIA
Keupayaan makmal memberikan perkhidmatan analisis adalah
parameter analisis yang diberikan agar keputusan yang
dikeluarkan adalah diterima sepenuhnya.
memerlukan pematuhan sepenuhnya bagi syarat-syarat yang ditetapkan oleh negara
pengimport. Ianya termasuk syarat akreditasi makmal yang menyediakan perkhidmatan
masa hadapan kemaskini keupayaan analisis dan status akreditasi yang terkandung di
dalam buku ini akan dimuatkan di laman web
Maklumat yang terkandung dalam buku ini adalah diharapkan dapat membantu program
negara ini adalah selamat untuk orang ramai.
NORAINI BT. DATO’ MOHD OTHMAN
Kementerian Kesihatan Malaysia
Perutusan Pengarah Kanan
ii
Perkhidmatan analisis yang ditawarkan
Makmal telah memperolehi akreditasi
KANDUNGAN
i
ii
Muka
surat
F
*
Sidang Pengarang
Perutusan Pengarah Kanan
1.0 Perkhidmatan Analisis dan Akreditasi
Petunjuk :
2
jad
ua
l 1
.1: p
er
kh
idm
ata
n a
na
lis
is -
resid
u d
ad
ah
DO
C.
NO
TE
ST
ME
TH
OD
R
EF
ER
EN
CE
PA
RA
ME
TE
RF
OO
D
MA
TR
IX
MIN
IMU
M
WE
IGH
T
LO
Q
(µg/k
g)
CO
NT
AIN
ER
TR
AN
SP
OR
TA
TIO
N
ST
OR
AG
E
MA
XIM
UM
PE
RM
ITT
ED
PR
OP
OR
TIO
N
(µg
/kg
)
MKAK
MKA IPOH
MKA JB
MKA KK
KUCHING
KEDAH
PERLIS
PULAU PINANG
SELANGOR
PAHANG
KELANTAN
TERENGGANU
Th
iab
en
da
zo
le5
Flu
be
nd
azo
le1
0
Su
lfa
me
razin
e2
0A
FA
FA
FA
Su
lfa
dim
idin
e4
0-5
0A
FA
FA
Pyrim
eth
am
ine
50
A
Su
lfa
mo
no
me
tho
xin
e3
0A
FA
FA
FA
Oxo
linic
acid
40
-50
AF
AA
FA
Su
lfa
dim
eth
oxin
e4
0A
FA
FA
FA
Difu
razo
ne
10
0A
FA
Su
lfa
qu
ino
xa
line
40
-50
AF
AF
AF
A
Nic
arb
azin
e2
0A
FA
AF
A
Su
lfa
dia
zin
e4
0A
FA
FA
FA
Su
lfa
thia
zo
le4
0A
FA
FA
Oxyte
tra
cyclin
e4
0A
FA
Te
tra
cyclin
e4
0A
FA
Ch
lort
etr
acyclin
e6
0A
FA
Do
xycyclin
e4
0A
FA
Fu
razo
lido
ne
me
tab
olit
e :
AO
ZA
FA
FA
FA
F
Fu
ralta
do
ne
me
tab
olit
e :
AM
OZ
AF
AF
AF
AF
Nitro
fura
nto
in m
eta
bo
lite
:
AH
DA
FA
FA
F
Nitro
fura
zo
ne
me
tab
olit
e :
SE
M
AF
AF
AF
Me
at
&
Me
at
Pro
du
cts
,
Fis
h &
Fis
h
Pro
du
cts
50
0 g
(ed
ible
po
rtio
n)
Pla
stic
50
0g
(ed
ible
po
rtio
n)
50
0g
(ed
ible
po
rtio
n)
Le
o M
.L.
No
llet.
20
00
.
Se
co
nd
Ed
itio
n.
Fo
od
An
aly
sis
by H
PL
C
Le
o M
.L.
No
llet.
20
00
.
Se
co
nd
Ed
itio
n.
Fo
od
An
aly
sis
by H
PL
C
AO
AC
99
5.0
5,
20
00
Jo
urn
al o
f
Ch
rom
ato
gra
ph
y A
,
93
9 (
20
01
)
2011
Re
fer
to
Fifte
en
th A
Sch
ed
ule
(Re
gu
latio
n 4
0)
D0
4-0
04
De
term
ina
tio
n o
f
Te
tra
cyclin
es in
An
ima
l
Tis
su
e b
y H
igh
P
erf
orm
an
ce
Liq
uid
Ch
rom
ato
gra
ph
y (
HP
LC
)
D0
4-0
09
De
term
ina
tio
n o
f
Nitro
fura
n M
eta
bo
lite
s in
Me
at
& M
ea
t P
rod
ucts
,
Fis
h &
Fis
h P
rod
ucts
by
Liq
uid
Ch
rom
ato
gra
ph
y
Ta
nd
em
Ma
ss
Sp
ectr
om
etr
y
De
term
ina
tio
n o
f
An
tib
acte
ria
ls in M
ea
t
an
d M
ea
t P
rod
ucts
an
d
Fis
h a
nd
Fis
h P
rod
ucts
by H
igh
Pe
rfo
rma
nce
Liq
uid
Ch
rom
ato
gra
ph
y
D0
4-0
02
D0
4-0
01
De
term
ina
tio
n o
f
An
the
lmin
tics in M
ea
t
an
d M
ea
t P
rod
ucts
an
d
Fis
h a
nd
F
ish
Pro
du
cts
by H
PL
C
Fro
ze
n
1
50
0g
(ed
ible
po
rtio
n)
3
jad
ua
l 1
.1: p
er
kh
idm
ata
n a
na
lis
is -
resid
u d
ad
ah
jad
ua
l 1
.1: p
er
kh
idm
ata
n a
na
lis
is -
resid
u d
ad
ah
jad
ua
l 1
.1: p
er
kh
idm
ata
n a
na
lis
is -
resid
u d
ad
ah
rk
hid
mat
rk
hid
mat
rk
hid
mat
dm
at
is -
resid
u d
ad
ah
is -
resid
u d
ad
ah
idu
da
da
hid
u d
ad
ah
idu
da
da
hid
u d
ad
ah
idu
da
da
hid
u d
ad
ah
idu
da
da
hid
u d
ad
ah
D0
4-0
10
De
term
ina
tio
n o
f
Ch
lora
mp
he
nic
ol in
Me
at
an
d M
ea
t P
rod
uct,
Fis
h
an
d F
ish
Pro
du
ct
by
Liq
uid
Ch
rom
ato
gra
ph
y
Ta
nd
em
Ma
ss
Sp
ectr
om
etr
y
Jo
urn
al o
f
Ch
rom
ato
gra
ph
y A
,
99
4 (
20
03
)
Ch
lora
mp
en
icol
Me
at
&
Me
at
Pro
du
cts
,
Fis
h &
Fis
h
Pro
du
cts
50
0 g
(ed
ible
po
rtio
n)
0.2
Pla
stic
Fro
ze
nA
FA
FA
FA
FA
F
Su
lfa
dia
zin
e
Su
lfa
thia
zo
le
Su
lfa
pyrid
ine
Su
lfa
me
razin
e
Su
lfa
dim
idin
e2
0
Su
lfa
mo
no
me
tho
xin
e4
0
Su
lfa
dim
eth
oxin
e2
0
Su
lfa
qu
ino
xa
line
40
D0
4-0
13
De
term
ina
tio
n o
f
Ch
lora
mp
he
nic
ol in
Ho
ne
y b
y L
iqu
id
Ch
rom
ato
gra
ph
y
Ta
nd
em
Ma
ss
Sp
ectr
om
etr
y
Po
ste
r B
10
5,
5th
Inte
rna
tio
na
l
Sym
po
siu
m o
n
Ho
rmo
ne
an
d
Ve
terin
ary
Dru
g
Re
sid
ue
An
aly
sis
,
An
twe
rp,
Belg
ium
,
Ma
y 1
6-1
9,
20
06
Ch
lora
mp
he
nic
ol
Ho
ne
y5
00
ml
0.0
5-0
.2
Am
be
r b
ott
le
/Com
merc
ial
Pa
ck
Ro
om
Te
mp
era
ture
A
D0
4-0
16
De
term
ina
tio
n o
f
Ch
lora
mp
he
nic
ol u
sin
g
Te
st
Kits (
Re
no
ge
nic
)
Kit In
str
uctio
nM
an
ua
lC
hlo
ram
ph
en
ico
l5
00
g0
.3-1
Pla
stic
Fro
ze
n
30
eg
gs
or
1kg
Ro
om
Te
mp
era
ture
Eg
g
50
0 g
Jo
urn
al o
f
Ch
rom
ato
gra
ph
y B
,
77
4 (
20
02
)
Kit In
str
uctio
nM
an
ua
lM
ea
t &
M
ea
tP
rod
ucts
,
Fis
h &
Fis
h
Pro
du
cts
De
term
ina
tio
n o
f B
eta
-
Ag
on
ist
usin
g T
est
Kits
(Re
no
ge
nic
)
1
Re
fer
to
Fifte
en
th A
Sch
ed
ule
(Re
gu
latio
n 4
0)
D0
4-0
15
D0
4-0
12
De
term
ina
tio
n o
f
An
tib
acte
ria
l R
esid
ue
s in
Eg
gs b
y H
igh
Pe
rfo
rma
nce
Liq
uid
Ch
rom
ato
gra
ph
y
Sa
lbu
tam
ol
Pla
stic /
Co
mm
erc
ial
Pa
ck
40
DO
C.
NO
TE
ST
ME
TH
OD
R
EF
ER
EN
CE
PA
RA
ME
TE
RF
OO
D
MA
TR
IX
MIN
IMU
M
WE
IGH
T
LO
Q
(µg/k
g)
CO
NT
AIN
ER
TR
AN
SP
OR
TA
TIO
N
ST
OR
AG
E
MA
XIM
UM
PE
RM
ITT
ED
PR
OP
OR
TIO
N
(µg
/kg
)
MKAK
MKA IPOH
MKA JB
MKA KK
KUCHING
KEDAH
PERLIS
PULAU PINANG
SELANGOR
PAHANG
KELANTAN
TERENGGANU
4
Alb
en
da
zo
le (
AL
B)
10
Ch
lora
mp
he
nic
ol (C
AP
)0
.2
Flo
rfe
nic
ol (F
F)
0.5
Oxfe
nd
azo
le (
OX
FE
N)
10
Su
lph
ad
imid
ine
(S
DD
)1
0
Su
lph
ad
ime
tho
xin
e (
SD
M)
5
Th
iab
en
da
zo
le (
TB
Z)
10
Th
iam
ph
en
ico
l (T
AP
)0
.5
D0
4-0
18
De
term
ina
tio
n o
f B
eta
-
Ag
on
ist
usin
g T
est
Kits
(Ra
nd
ox)
Kit In
str
uctio
nM
an
ua
lS
alb
uta
mo
l5
00
g1
Pla
stic
Fro
ze
n
Cle
nb
ute
rol
Cim
ate
rol
Ma
bu
tero
l
Te
rbu
talin
e
Ra
cto
pa
min
e
Sa
lbu
tam
ol
Ma
lach
ite
Gre
en
AF
AF
Le
uco
ma
lach
ite
Gre
en
AF
Cry
sta
l V
iole
tA
F
Le
ucry
sta
l V
iole
t
Fu
razo
lido
ne
me
tab
olit
e :
AO
Z
Fu
ralta
do
ne
me
tab
olit
e :
AM
OZ
Co
mm
erc
ial
Pa
ck o
r
Pla
stic
Ch
ille
d /
Ro
om
Te
mp
era
ture
Milk
50
0 m
l o
r
50
0 g
1
De
term
ina
tio
n o
fT
rip
he
nylm
eth
an
e D
ye
sin
Me
at
an
d M
ea
tP
rod
ucts
an
d F
ish
an
d
Fis
h P
rod
ucts
by L
iqu
idC
hro
ma
tog
rap
hy
Ta
nd
em
Ma
ss
Sp
ectr
om
etr
y
D0
4-0
20
(a
) A
na
lytica
Ch
imic
a
Acta
58
6 (
20
07
)
(b)
J.
Ag
ric F
oo
d
Ch
em
istr
y
Kit In
str
uctio
nM
an
ua
l
Me
at
&
Me
at
Pro
du
cts
,
Fis
h &
Fis
h
Pro
du
cts
Fro
ze
n
SO
P A
RO
/48
0 (
20
05
),
Na
tio
na
l P
ub
lic H
ea
lth
an
d E
nviro
nm
en
t,
Ne
the
rla
nd
s,
D0
4-0
17
De
term
ina
tio
n o
fM
ulti
Re
sid
ue
of
Ve
teri
na
ry
Dru
g in
Milk
by L
iqu
id
Ch
rom
ato
gra
ph
y M
ass
Sp
ectr
om
etr
y a
nd
Ta
nd
em
Ma
ss
Sp
ectr
om
etr
y
Jo
urn
al o
f
Ch
rom
ato
gra
ph
y A
,
12
05
(2
00
8)
50
0 g
(ed
ible
p
ort
ion
)
50
0 g
(ed
ible
po
rtio
n)
50
0g
(ed
ible
po
rtio
n)
50
Pla
stic
D0
4-0
19
De
term
ina
tio
n o
f B
eta
-
Ag
on
ist
in M
ea
t &
Me
at
Pro
du
ct,
Fis
h &
Fis
h
Pro
du
ct
by L
iqu
id
Ch
rom
ato
gra
ph
y
Ta
nd
em
Ma
ss
Sp
ectr
om
etr
y
Pla
stic
Pla
stic
Fro
ze
n
Fro
ze
n
1
D0
4-0
21
De
term
ina
tio
n o
f
Nitro
fura
n (
AM
OZ
&
AO
Z)
usin
g B
ioo
Scie
ntific T
est
Kit
DO
C.
NO
TE
ST
ME
TH
OD
R
EF
ER
EN
CE
PA
RA
ME
TE
RF
OO
D
MA
TR
IX
MIN
IMU
M
WE
IGH
T
LO
Q
(µg/k
g)
CO
NT
AIN
ER
TR
AN
SP
OR
TA
TIO
N
ST
OR
AG
E
MA
XIM
UM
PE
RM
ITT
ED
PR
OP
OR
TIO
N
(µg
/kg
)
MKAK
MKA IPOH
MKA JB
MKA KK
KUCHING
KEDAH
PERLIS
PULAU PINANG
SELANGOR
PAHANG
KELANTAN
TERENGGANU
jad
ua
l 1
.1: p
er
kh
idm
ata
n a
na
lis
is -
resid
u d
ad
ah
jad
ua
l 1
.1: p
er
kh
idm
ata
n a
na
lis
is -
resid
u d
ad
ah
jad
ua
l 1
.1: p
er
kh
idm
ata
n a
na
lis
is -
resid
u d
ad
ah
is -
resid
u d
ad
ah
is -
resid
u d
ad
ah
idu
da
da
hid
u d
ad
ah
idu
da
da
hid
u d
ad
ah
idu
da
da
hid
u d
ad
ah
idu
da
da
h
5
2-a
min
o-a
lbe
nd
azo
le
sulfo
ne
(2
AA
)A
FA
FA
F
Alb
endazole
sulfone (A
SF
) A
FA
FA
F
Fe
nb
en
da
zo
le (
FE
N)
AF
AF
AF
Oxfe
nd
azo
le (
OX
FE
N)
AF
AF
AF
Th
iab
en
da
zo
le (
TB
Z)
AF
AF
AF
AF
AF
Alb
en
da
zo
le (
AL
B)
AF
AF
AF
AF
Flu
be
nd
azo
le (
FL
UB
)A
FA
FA
FA
FA
F
Me
be
nd
azo
le (
ME
B)
AF
AF
AF
Alb
en
da
zo
le S
ulfo
xid
e
(AS
OX
)A
FA
FA
FA
F
Fe
ba
nte
l (F
EB
AN
)A
FA
FA
F
Dim
etr
ida
zo
le m
eta
bo
lite
s
(HM
MN
I)1
AF
Me
tro
nid
azo
le (
MN
Z)
AF
Ro
nid
azo
le (
RN
Z)
AF
Cip
roflo
xa
cin
En
roflo
xa
cin
Diflo
xa
cin
Sa
raflo
xa
cin
Da
no
flo
xa
cin
10
Ma
rbo
flo
xa
cin
2
No
rflo
xa
cin
Oxolin
ic a
cid
50.5
Jo
urn
al o
fC
hro
ma
tog
rap
hy A
,
88
2 (
20
00
)
(a
) L
eo
M.L
. N
olle
t.
20
00
. S
eco
nd
Ed
itio
n.
Fo
od
An
aly
sis
by
HP
LC
(b)
Jo
urn
al o
f
Ch
rom
ato
gra
ph
y,
49
8 (
19
90
)
1D
04
-02
2
De
term
ina
tio
n o
f
Be
nzim
ida
zo
le R
esid
ue
s
in F
ish
an
d F
ish
Pro
du
cts
by L
iqu
id
Ch
rom
ato
gra
ph
y
Ta
nd
em
Ma
ss
Sp
ectr
om
etr
y
Th
e D
ete
rmin
atio
n o
f
Nitro
imid
azo
le R
esid
ue
s
in F
ish
an
d F
ish
Pro
du
cts
by L
iqu
id
Ch
rom
ato
gra
ph
y
Ta
nd
em
Ma
ss
Sp
ectr
om
etr
y
Re
fer
toF
ifte
en
th A
S
ch
ed
ule
(Re
gu
latio
n 4
0)
Re
fer
to
Fifte
en
th A
S
ch
ed
ule
(Re
gu
latio
n 4
0)
Pla
stic
Fro
ze
n
5u
g/k
g
50
0g
(ed
ible
po
rtio
n)
D0
4-0
26
De
term
ina
tio
n o
f
Qu
ino
lon
es a
nd
Flu
oro
qu
ino
lon
es
Re
sid
ue
s In
Me
at
an
d
Me
at
Pro
du
ct
an
d F
ish
an
d F
ish
Pro
du
cts
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y
Ta
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em
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ss
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r T
he
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ar
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20
10
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23
Me
at
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at
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du
cts
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Fis
h &
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h
Pro
du
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5
DO
C.
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TE
ST
ME
TH
OD
R
EF
ER
EN
CE
PA
RA
ME
TE
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OO
D
MA
TR
IX
MIN
IMU
M
WE
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T
LO
Q
(µg/k
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CO
NT
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ER
TR
AN
SP
OR
TA
TIO
N
ST
OR
AG
E
MA
XIM
UM
PE
RM
ITT
ED
PR
OP
OR
TIO
N
(µg
/kg
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MKA IPOH
MKA JB
MKA KK
KUCHING
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jad
ua
l 1
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er
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er
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ua
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er
kh
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resid
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u d
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ah
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da
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da
da
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6
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AP
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F)
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AF
Th
iam
ph
en
ico
l (T
AP
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F
D0
4-0
27
De
term
ina
tio
n o
f
Ph
en
ico
l R
esid
ue
s in
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at
an
d M
ea
t P
rod
ucts
an
d F
ish
an
d F
ish
Pro
du
cts
by L
iqu
id
Ch
rom
ato
gra
ph
y
Ta
nd
em
Ma
ss
Sp
ectr
om
etr
y
Me
at
an
d
Me
at
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du
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an
d F
ish
an
d F
ish
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du
cts
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ible
Po
rtio
n)
Pla
stic
Fro
ze
n
Jo
urn
al o
f
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rom
ato
gra
ph
y B
,
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20
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fer
to
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th A
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gu
latio
n 4
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DO
C.
NO
TE
ST
ME
TH
OD
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EF
ER
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CE
PA
RA
ME
TE
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D
MA
TR
IX
MIN
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M
WE
IGH
T
LO
Q
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CO
NT
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ER
TR
AN
SP
OR
TA
TIO
N
ST
OR
AG
E
MA
XIM
UM
PE
RM
ITT
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PR
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OR
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N
(µg
/kg
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MKAK
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MKA KK
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7
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dit
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ak
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DO
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TE
ST
ME
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OD
RE
FE
RE
NC
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AR
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OD
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NT
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ER
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E
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alit
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st
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ric
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an
d B
ora
tes in
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od
AO
AC
, V
ol. II (1
99
5),
Ch
ap
ter
47
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ric
Acid
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od
le /
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ey
teo
w /
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h b
all
/
Fis
h c
ake
/Oth
er
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ds
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0g
10
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/kg
pla
stic
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ina
l
pa
cka
gin
g
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t p
erm
itte
dA
FA
AF
AA
AA
AA
A
E0
4-0
02
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e D
ete
rmin
atio
n o
f
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nzo
ic A
cid
an
d S
orb
ic
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in
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od
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g L
iqu
id
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rom
ato
gra
ph
y
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tern
al S
td)
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od
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c.
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. A
na
l.
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em
. 7
0 (
5)
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nzo
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rbic
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ffo
od
25
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stic /
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ss /
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ttle
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rig
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l
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cka
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fer
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g.
20
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AA
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rmit
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lou
r
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ra R
ed A
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ara
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ino
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fer
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oo
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eg
ula
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ns
19
85
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ure
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00
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AA
AA
A
Jo
urn
al o
f C
he
mic
al
Ed
uca
tio
n,
19
85
,
Vo
l. 6
2 ,
No
5
Fd
. C
he
m T
oxic
olo
gy
Vo
l. 2
7,
No
. 1
Air tig
ht
co
nta
ine
r /
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gin
al
Pa
cka
gin
g
As P
urc
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se
25
0 g
per
co
lou
rE
04
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4-0
04
All
typ
es o
ffo
od
AO
AC
(1
97
50
).
12
th e
ditio
n.
Ch
ap
ter
34
20
0-5
00
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/kg
50
0g
Ori
gin
al
Pa
cka
gin
gA
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e D
ete
rmin
atio
n o
fW
ate
r
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lub
le S
yn
the
tic F
oo
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Co
lou
r in
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od
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rom
ato
gra
ph
y P
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er
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d
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ectr
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r
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e D
ete
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od
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y L
iqu
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rom
ato
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t A
va
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T)
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bite
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lour
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ra R
ed
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eth
yl Y
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da
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da
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da
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6 m
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da
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Perm
itted C
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ur
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ra R
ed A
C
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ara
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t B
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oco
late
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wn
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Ery
thro
sin
e B
S
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st
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en
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Gre
en
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igo
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e
Po
nce
au
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nse
t Y
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CF
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rtra
zin
e
Qu
ino
line
Ye
llow
No
t A
va
ilab
le
A
(a)
AO
AC
Off
icia
l M
eth
od
98
3.1
5,
Ch
.47
(b)
AO
AC
In
tern
atio
na
l,
16
th E
ditio
n,
Vo
lum
eII,
19
96
E0
4-0
05
Th
e D
ete
rmin
atio
n o
f
Syn
the
tic A
ntio
xid
an
ts
(BH
A &
BH
T)
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ats
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ils,
an
d B
utt
er
Oil
by H
igh
Pe
rfo
rma
nce
Liq
uid
Ch
rom
ato
gra
ph
y
E0
4-0
06
25
0g
10
mg
/kg
10
mg
/kg
Pla
stic /
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gin
al
Pa
cka
gin
g
Re
fer
to
Ta
ble
1 1
0th
Sch
ed
ule
(re
g.
24
)
(a)
AS
TA
(Am
erica
n S
pic
e
Tra
de
Asso
cia
tio
n)
20
05
(b)
Yo
shio
ka (
2008)
-
Ta
lan
ta.
Vol. 7
4
De
term
ina
tio
n o
f S
yn
the
tic
Co
lou
r in
Fo
od
Usin
g L
iqu
id
Ch
rom
ato
gra
ph
y
Ed
ible
Fa
t a
nd
Ed
ible
Oil
All
typ
es o
ffo
od
50
0g
As P
urc
ha
se
DO
C.
NO
TE
ST
ME
TH
OD
RE
FE
RE
NC
EP
AR
AM
ET
ER
FO
OD
MA
TR
IXM
INIM
UM
WE
IGH
TL
OQ
CO
NT
AIN
ER
TR
AN
SP
OR
TA
TIO
N
ST
OR
AG
E
MA
XIM
UM
PE
RM
ITT
ED
PR
OP
OR
TIO
N
MKAK
MKA IPOH
MKA JB
MKA KK
KUCHING
KEDAH
PERLIS
PULAU PINANG
SELANGOR
PAHANG
KELANTAN
TERENGGANU
jad
ua
l 1
.2: a
dit
if m
ak
an
an
9
E0
4-0
10
Th
e D
ete
rmin
atio
n o
f
So
diu
m C
hlo
rid
e in
Sa
lte
d
Fo
od
s b
y U
sin
g V
olh
ard
Me
tho
d
De
term
ina
tio
n o
f S
ma
ll
Am
ou
nt
of
Ch
lori
de
by
Vo
lha
rd T
itra
tio
n,
19
59
Sa
lt C
on
ten
tA
ll ty
pe
s o
f
sa
lte
dfo
od
25
0g
No
t
Ava
ilab
le
Re
fer
to F
oo
d
Re
gu
latio
ns
19
85
E0
4-0
11
Th
e D
ete
rmin
atio
n o
f
Fo
rma
lde
hyd
e In
Fis
h M
ea
t
Usin
g S
am
ple
Pre
pa
ratio
n
Me
tho
d A
OA
C 9
31
.08
Fo
llow
Qu
an
tita
tio
n U
sin
g
Na
sh
's R
ea
ge
nt
AO
AC
Off
icia
l M
eth
od
93
1.0
8.
17
th e
ditio
n.
Vo
l.II.
Ch
ap
ter
47
Fo
rma
lde
hyd
eF
ish
& F
ish
Pro
du
cts
1kg
1 m
g/k
gF
roze
n
Ad
min
istr
ative
leve
l: 5
mg
/kg
for
pa
sta
an
d
20
mg
/kg
fo
r
fish
Pla
stic /
Ori
gin
al
Pa
cka
gin
g
Sa
cch
arin
Pe
rmitte
d
on
ly in
dri
ed
fru
it,
dri
ed
pre
pa
red
fis
h
& d
rie
d v
eg
.
Cycla
ma
teN
ot
pe
rmitte
d
Sa
cch
arin
10
-80
mg
/kg
Pe
rmitte
d
on
ly in
dri
ed
fru
it,
dri
ed
pre
pa
red
fis
h
& d
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eg
.
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ma
te4
0-1
00
mg
/kg
No
t p
erm
itte
d
Su
lfu
r D
ioxid
e
( q
ua
lita
tif)
Su
lfu
r D
ioxid
e
( q
ua
ntita
tif)
AO
AC
(1
99
0)
Vo
l. 1
1
A AF
A
AA
A
AA
A
AA
AA
AA
Pla
stic /
Ori
gin
al
Pa
cka
gin
g
Re
fer
to
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ble
1
(Re
g.
20
)
As P
urc
ha
se
Pla
stic /
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gin
al
Pa
cka
gin
g
10 m
g/k
g5
00
gE
04
-00
9
25
0g
All
typ
es o
ffo
od
25
0g
E0
4-0
08
E0
4-0
07
All
typ
es o
ffo
od
Th
e D
ete
rmin
atio
n o
f
Su
lph
ur
Dio
xid
e in
Fo
od
by
Titra
tio
n
JA
OA
C (
La
wre
nce
et
al)
Vo
l. 7
1,
No
5,
19
88
AO
AC
Off
icia
l M
eth
od
96
1.0
9.
17
th e
ditio
n.
Vo
l.II.
Ch
ap
ter
47
Th
e D
ete
rmin
atio
n o
f
Sa
cch
arin
an
d C
ycla
ma
te
in F
oo
d b
y T
hin
La
ye
r
Ch
rom
ato
gra
ph
y
25
-10
0
mg
/kg
A
Th
e D
ete
rmin
atio
n o
f
Sa
cch
arin
an
d C
ycla
ma
te
in F
oo
d u
sin
g L
iqu
id
Ch
rom
ato
gra
ph
y
A
DO
C.
NO
TE
ST
ME
TH
OD
RE
FE
RE
NC
EP
AR
AM
ET
ER
FO
OD
MA
TR
IXM
INIM
UM
WE
IGH
TL
OQ
CO
NT
AIN
ER
TR
AN
SP
OR
TA
TIO
N
ST
OR
AG
E
MA
XIM
UM
PE
RM
ITT
ED
PR
OP
OR
TIO
N
MKAK
MKA IPOH
MKA JB
MKA KK
KUCHING
KEDAH
PERLIS
PULAU PINANG
SELANGOR
PAHANG
KELANTAN
jad
ua
l 1
.2: a
dit
if m
ak
an
an
10
E0
4-0
13
Th
e D
ete
rmin
atio
n o
f
Po
tassiu
m B
rom
ate
s in
Flo
ur
an
d F
lou
r P
rod
ucts
Bro
ma
tes a
nd
Io
da
tes in
Wh
ite
an
d W
ho
le W
he
at
Flo
ur,
AO
AC
Off
icia
l
Me
tho
d 9
56
.03
,
AO
AC
O
ffic
ial M
eth
od
of
An
aly
sis
19
95
Po
tassiu
m b
rom
ate
E0
4-0
14
Th
e D
ete
rmin
atio
n o
f O
il
So
lub
le S
yn
the
tic F
oo
d
Co
lou
rs (
Su
da
n I &
IV
) in
foo
d b
y P
ap
er
Ch
rom
ato
gra
ph
y a
nd
UV
/VIS
Sp
ectr
op
ho
tom
ete
r
AO
AC
(1
99
1)
Off
icia
l
Me
tho
ds o
f A
na
lysis
of
AO
AC
In
tern
atio
na
l
Su
da
n I &
IV
)A
E0
4-0
16
Ra
pid
Me
tho
d f
or
Diffe
ren
tia
tio
n o
f G
en
uin
e
an
d Im
ita
tio
n S
ha
rks F
in
Ch
ew
, S
.T.
et
al (1
99
2);
Sin
ga
po
re J
ou
rna
l o
f
Pro
ma
ryIn
du
str
y 2
0 (
2)
Sh
ark
s F
inF
ish
10 m
g/k
g
E0
4-0
17
Th
e D
ete
rmin
atio
n o
f
Pe
rce
nta
ge
So
lub
le S
olid
in
Fo
od
by R
efr
acto
me
try
Inte
rna
tio
na
l T
em
pe
ratu
re
Co
rre
ctio
n T
ab
le,
19
36
.
Int.
Su
ga
r J.
39
, 2
4s,1
93
7
Pe
rce
nta
ge
So
lub
le S
olid
All
typ
es o
ffo
od
Re
fer
to F
oo
d
Re
gu
latio
ns
19
85
E0
4-0
18
Th
e D
ete
rmin
atio
n o
f N
et
Co
nte
nt
in C
an
ne
d P
rod
uct
by D
rain
ed
We
igh
t M
eth
od
La
wre
nce
, J
.F.,
JA
OA
C,
Vo
l 7
1,
No
5,
19
88
Ne
t C
on
ten
tC
an
ne
d F
ish
2 c
an
sN
ot
less t
ha
n
55
% F
ish
A
E0
4-0
19
Th
e M
ea
su
rem
en
t o
fIo
din
e
Co
nte
nt
in Io
dis
ed
Sa
lt
De
Ma
eye
r E
M,
Lo
we
nste
in
FW
and T
hill
y C
H -
“T
he
Co
ntr
ol o
f
En
de
mic
Go
ite
r"
WH
O,
Ge
ne
va
, 1
97
9
Iod
ine
Co
nte
nt
Sa
lt2
50
g1
5 m
g/k
g2
0 -
30
mg
/kg
AA
A
All
typ
es o
ffo
od
Pla
stic /
Ori
gin
al
Pa
cka
gin
g
As P
urc
ha
se
No
t A
va
ilab
le
No
t
Ava
ilab
le
25
0g
DO
C.
NO
TE
ST
ME
TH
OD
RE
FE
RE
NC
EP
AR
AM
ET
ER
FO
OD
MA
TR
IXM
INIM
UM
WE
IGH
TL
OQ
CO
NT
AIN
ER
TR
AN
SP
OR
TA
TIO
N
ST
OR
AG
E
MA
XIM
UM
PE
RM
ITT
ED
PR
OP
OR
TIO
N
MKAK
MKA IPOH
MKA JB
MKA KK
KUCHING
KEDAH
PERLIS
PULAU PINANG
SELANGOR
PAHANG
KELANTAN
TERENGGANU
jad
ua
l 1
.2: a
dit
if m
ak
an
an
11
E0
4-0
20
Th
e D
ete
rmin
atio
n o
fIo
din
e
Co
nte
nt
in Io
dis
ed
Sa
lt
Usin
g Io
do
me
tric
Titra
tio
n
(Pe
ars
on
)
Th
e C
he
mic
al A
na
lysis
of
Fo
od
s,
8th
Ed
itio
n
Iod
ine
Co
nte
nt
Sa
lt2
0 m
g/k
g2
0 -
30
mg
/kg
AA
E0
4-0
22
Th
e D
ete
rmin
atio
n o
f
Pe
roxid
e v
alu
e
MP
OB
Te
st
Me
tho
d
p2
:3 :
20
04
- P
ero
xid
e V
alu
e
Pe
roxid
e V
alu
eE
dib
le O
il &
Fat
/ O
ily F
oo
d
No
t
Ava
ilab
le1
0 m
eq
/kg
E0
4-0
24
Th
e D
ete
rmin
atio
n o
f A
cid
Va
lue
MP
OB
Te
st
Me
tho
d
c2
.7:2
00
4 A
cid
Va
lue
:
Fa
tty A
cid
Acid
Va
lue
Re
fer
to F
oo
d
Re
gu
latio
ns
19
85
E0
4-0
25
Th
e D
ete
rmin
atio
n o
f A
ce
tic
Acid
Ha
rold
Eg
an
et
al.,
Pe
ars
on
's
Ch
em
ica
l
An
aly
sis
of
Fo
od
s.1
981
8th
Ed
itio
n
Ace
tic A
cid
Asp
art
am
e2
50
g/m
l1
00
mg
/kg
Ph
en
yla
lan
ine
25
0g
/ml
10
mg
/kg
(a)
Jo
urn
al o
f F
oo
d
Hyg
ien
e S
ocie
ty o
f Ja
pa
n,
Vo
l. 3
3:
, 1
99
2.
(b)
Ra
pid
An
aly
sis
Me
tho
ds
for
Pe
sticid
e R
esid
ue
s,
Hyg
ien
e a
nd
Ch
em
istr
y,
No
. 4
8,
Ap
ril 8
,19
97
.
As P
urc
ha
se
De
term
ina
tio
n o
f
Asp
art
am
e a
nd
Ph
en
yla
lan
ine
in
So
ft D
rink
by H
igh
Pe
rfo
rma
nce
Liq
uid
Ch
rom
ato
gra
ph
y
E0
4-0
26
Pla
stic /
Ori
gin
al
Pa
cka
gin
g
A
25
0g
So
ft D
rin
k
No
t
Ava
ilab
le2
50
gE
dib
le O
il &
Fat
/ O
ily F
oo
d
No
t A
va
ilab
le
DO
C.
NO
TE
ST
ME
TH
OD
RE
FE
RE
NC
EP
AR
AM
ET
ER
FO
OD
MA
TR
IXM
INIM
UM
WE
IGH
TL
OQ
CO
NT
AIN
ER
TR
AN
SP
OR
TA
TIO
N
ST
OR
AG
E
MA
XIM
UM
PE
RM
ITT
ED
PR
OP
OR
TIO
N
MKAK
MKA IPOH
MKA JB
MKA KK
KUCHING
KEDAH
PERLIS
PULAU PINANG
SELANGOR
PAHANG
KELANTAN
TERENGGANU
jad
ua
l 1
.2: a
dit
if m
ak
an
an
12
E0
4-0
31
Th
e D
ete
rmin
atio
n o
f
Synth
etic A
ntioxid
ant
(PG
, T
BH
Q, B
HA
& B
HT
) in
Ed
ible
Oil
by H
igh
Pe
rfo
rma
nce
Liq
uid
Ch
rom
ato
gra
ph
y
Ma
gd
a R
afe
ca
s,
Fra
nce
sc
Gu
ard
iola
, M
iqu
ei Ille
ra,
Ra
fae
l C
od
on
y &
Jo
se
ph
Bo
ate
lla.
(19
98
).
Jo
urn
al o
f
Ch
rom
ato
gra
ph
y A
Syn
the
tic
An
tio
xid
an
tE
dib
le O
il 2
50
gN
ot
Ava
ilab
le
Re
fer
to
Ta
ble
1,
10
th
Sch
ed
ule
(Re
g.
24
)
As P
urc
ha
se
Pla
stic /
Ori
gin
al
Pa
cka
gin
g
Lo
w e
ne
rgy
so
ft d
rin
k -
60
0 m
g/L
,
Oth
er
low
en
erg
y f
oo
d
30
00
mg
/kg
E0
4-0
28
Th
e D
ete
rmin
atio
n o
f
Su
lph
ur
Dio
xid
e in
Fo
od
An
aly
sis
for
To
tal S
ulp
hite
s
in F
oo
ds b
y u
sin
g r
ap
id
Dis
tilla
tio
n f
ollo
we
d b
y
Re
do
x T
itra
tio
n .
De
Vri
es
et
al. J
AO
AC
V
ol 6
9.
No
5,1
98
6
Su
lfu
r D
ioxid
e
A
ll ty
pe
s o
ffo
od
50
0g
AA
E0
4-0
29
Th
e D
ete
rmin
atio
n o
f
Su
lph
ur
Dio
xid
e in
Fo
od
Mo
nie
r W
illia
ms
(a)
Eg
an
,H e
t a
l.(1
98
1)
Pe
ars
on
's C
he
mic
al
An
aly
sis
of
Fo
od
(8
th.E
d)
(b
) A
OA
C 1
6th
Ed
.,
Vo
l .II (1
99
5),
AO
AC
Off
icia
l M
eth
od
93
2.1
6,
Ch
ap
.47
Su
lfu
r D
ioxid
eA
ll ty
pe
s o
ffo
od
50
0g
AF
A
E0
4-0
30
Th
e D
ete
rmin
atio
n o
f
Pro
pio
nic
Acid
In F
lou
r
Co
nfe
ctio
n
AO
AC
Vo
l 6
4,
No
. 2
,
19
81
Pro
pio
nic
Acid
Bre
ad
an
d F
lou
r
Co
nfe
ctio
ne
ry2
50
g4
00
mg
/kg
20
00
mg
/kg
AA
As P
urc
ha
se
Re
fer
to
Ta
ble
1
(Re
g.
20
)
Pla
stic /
Ori
gin
al
Pa
cka
gin
g
25
0g
/ml
No
t
Ava
ilab
le
E0
4-0
27
De
term
ina
tio
n o
f
Ace
su
lfa
me
K u
sin
g
by
Hig
h P
erf
orm
an
ce
Liq
uid
Ch
rom
ato
gra
ph
y
Ace
su
lfa
me
Po
tassiu
mB
eve
rag
es
Eu
rop
ea
n
Sta
nd
ard
EN
12
86
5
DO
C.
NO
TE
ST
ME
TH
OD
RE
FE
RE
NC
EP
AR
AM
ET
ER
FO
OD
MA
TR
IXM
INIM
UM
WE
IGH
TL
OQ
CO
NT
AIN
ER
TR
AN
SP
OR
TA
TIO
N
ST
OR
AG
E
MA
XIM
UM
PE
RM
ITT
ED
PR
OP
OR
TIO
N
MKAK
MKA IPOH
MKA JB
MKA KK
KUCHING
KEDAH
PERLIS
PULAU PINANG
SELANGOR
PAHANG
KELANTAN
TERENGGANU
jad
ua
l 1
.2: a
dit
if m
ak
an
an
13
Nirite
Nitra
te
E0
4-0
33
Th
e D
ete
rmin
atio
n o
f
Me
lam
ine
in
Fo
od
by L
iqu
id
Ch
rom
ato
gra
ph
y T
an
de
m
Ma
ss S
pe
ctr
om
etr
y
(LC
-MS
/MS
)
US
DA
/CF
SA
N.
20
07
.
La
bo
rato
ryIn
form
atio
n
Bu
lletin
No
. 4
39
6,
Vo
lum
e 2
3
Me
lam
ine
All
typ
es o
f fo
od
25
0g
0.0
1
mg
/kg
No
t P
erm
itte
dA
E0
4-0
34
De
term
ina
tio
n o
f
Fo
rma
lde
hyd
e in
Fis
h &
Fis
h P
rod
ucts
an
d P
asta
usin
g N
ash
'sM
eth
od
Be
nja
ku
l e
t.a
l. F
oo
d
Hyd
roco
lloid
s 1
9(2
00
5)
Fo
rma
lde
hyd
eF
ish
an
d F
ish
Pro
du
cts
1 k
g8
.5
mg
/kg
No
t A
va
ilab
le
E0
4-0
36
De
term
ina
tio
n o
f C
itra
te in
Fis
h a
nd
Fis
h P
rod
ucts
usin
g Io
n C
hro
ma
tog
rap
hy
US
En
vir
on
me
nta
l
Pro
tectio
n A
ge
ncy
(EP
A M
eth
od
90
56
A),
Re
v.
, 1
No
v.
20
00
Citra
teF
ish
an
d F
ish
Pro
du
cts
30
0g
25
mg
/kg
No
t A
vaila
ble
AF
Fo
od
Re
gu
latio
ns
19
85
(1
47
) :
EU
reg
ula
tio
ns:
Su
rim
i:
10
00
mg
/kg
,
Oth
er
Fis
h
Pro
du
cts
:
50
00
mg
/kg
As P
urc
ha
se
Pla
stic /
Ori
gin
al
Pa
cka
gin
gF
roze
n
US
En
vir
on
me
nta
l
Pro
tectio
n A
ge
ncy
(EP
A M
eth
od
90
56
A),
Re
v.
1,
No
v.
20
00
E0
4-0
32
De
term
ina
tio
n o
f N
itri
te a
nd
Nitra
te in
Me
at
Pro
du
ct
usin
g Io
n C
hro
ma
tog
rap
hy
Me
at
an
d M
ea
t
Pro
du
cts
30
0g
30
0g
37
5
mg
/kg
Fro
ze
n
50
mg
/kg
20
0 m
g/k
g
To
tal N
itrite
&
Nitra
te
ca
lcu
late
d a
s
Na
triu
m N
itrite
E0
4-0
38
De
term
ina
tio
n o
f
Po
lyp
ho
sp
ha
te in
Fis
h a
nd
Fis
h P
rod
ucts
usin
g Io
n
Ch
rom
ato
gra
ph
y
Po
lyp
ho
sp
ha
teF
ish
an
d F
ish
Pro
du
cts
US
En
vir
on
me
nta
l
Pro
tectio
n A
ge
ncy
(EP
A M
eth
od
90
56
A),
Re
v.
1,
No
v.
20
00
AF
DO
C.
NO
TE
ST
ME
TH
OD
R
EF
ER
EN
CE
PA
RA
ME
TE
RF
OO
D M
AT
RIX
MIN
IMU
M
WE
IGH
TL
OQ
CO
NT
AIN
ER
TR
AN
SP
OR
TA
TIO
N
ST
OR
AG
E
MA
XIM
UM
PE
RM
ITT
ED
PR
OP
OR
TIO
N
MKAK
MKA IPOH
MKA JB
MKA KK
KUCHING
KEDAH
PERLIS
PULAU PINANG
SELANGOR
PAHANG
KELANTAN
TERENGGANU
jad
ua
l 1
.2: a
dit
if m
ak
an
an
14
jad
ua
l 1
.3
resid
u r
ac
un
per
osa
k
DO
C.
NO
TE
ST
ME
TH
OD
GROUPR
EF
ER
EN
CE
PA
RA
ME
TE
RF
OO
DM
AT
RIX
MIN
IMU
M
WE
IGH
TL
OQ
(m
g/k
g)
C
ON
TA
INE
RT
RA
NS
PO
RT
AT
ION
ST
OR
AG
E
MA
XIM
UM
RE
SID
UE
LIM
ITS
(MR
Ls)
in f
oo
d
(mg
/kg
)
MKAK
MKA IPOH
MKA JB
MKA KK
KUCHING
KEDAH
PERLIS
PULAU PINANG
SELANGOR
PAHANG
KELANTAN
TERENGGANU
Azin
ph
os e
thyl
0.0
25
AA
Ca
rbo
fen
oth
ion
0.1
AA
AA
Ch
lorp
yri
ph
os
0.0
25
AA
AA
A
Ch
lorp
yrifo
s m
eth
yl
0.0
25
AA
AA
A
Cya
no
fen
ph
os
0.0
25
AA
AA
A
Dia
zin
on
0.0
1A
AA
AA
Dic
hlo
rvo
s0
.02
5A
AA
A
Dim
eth
oa
te0
.02
5
Eth
ion
0.0
25
AA
AA
A
Fe
nitro
thio
n0
.02
5A
AA
Fe
nsu
lfo
thio
n0
.01
Fe
nth
ion
0.0
25
A
Fo
rmo
thio
n0
.02
5A
AA
Ma
lath
ion
0.0
2A
AA
AA
Me
tha
mid
op
ho
s0
.02
5
Me
thid
ath
ion
0.0
1A
AA
Pa
rath
ion
eth
yl
0.0
5A
AA
Pa
rath
ion
me
thyl
0.0
5A
AA
Ph
osa
lon
e0
.05
AA
A
Pirim
iph
os m
eth
yl
0.0
1A
AA
AA
Pro
fen
op
ho
s0
.02
5A
AA
AA
Pro
thio
ph
os
0.0
25
AA
AA
Qu
ina
lph
os
0.0
2A
AA
AA
To
lclo
ph
os m
eth
yl
0.0
25
AA
AA
A
Jo
urn
al o
f F
oo
d H
yg
ien
e
So
cie
ty o
f Ja
pa
n,
Vo
l.
44
, N
o.
5
Re
fer
to
Six
tee
nth
Sch
ed
ule
(Re
gu
latio
n
41
)
Organophosporus
F0
4-0
01
Mu
ltip
le
Sim
ulta
ne
ou
s
Me
tho
d f
or
Pe
sticid
e
Re
sid
ue
s in
Fru
its
an
d V
eg
eta
ble
s
Fre
sh
Fru
its &
Ve
ge
tab
les
1 k
gA
mb
ien
t
Te
mp
era
ture
Bro
wn
pa
pe
r /
pla
stic
15
jad
ua
l 1
.3
resid
u r
ac
un
per
osa
k
2,4
-DD
T0
.02
5A
4,4
-DD
D0
.02
5A
4,4
-DD
E0
.02
5A
4,4
-DD
T0
.02
5A
Ald
rin
0.0
25
Ca
pta
fol
0.2
5
Ca
pta
n0
.25
Dic
hlo
ran
0.0
15
A
Die
ldrin
0.0
1A
En
drin
0.0
1A
Gam
ma-H
CH
/
Lin
da
ne
0.0
5A
He
pta
ch
lor
0.0
05
A
Qu
into
ze
ne
0.0
05
A
Tria
de
me
fon
0.0
5
Triflu
mu
ron
0.5
A
Cyflu
thrin
0.2
5A
Cyp
erm
eth
rin
0.0
5A
Fe
nva
lera
te0
.05
A
Pe
rme
thrin
0.0
25
A
Be
nd
ioca
rb0
.02
Ca
rba
ryl
0.2
Ca
rbo
fura
n0
.1
Fe
no
bu
ca
rb0
.12
5
Me
pro
nil
0.5
Pro
po
xu
r0
.25
Th
iob
en
ca
rb0
.01
Jo
urn
al o
f F
oo
d H
yg
ien
e
So
cie
ty o
f Ja
pa
n,
Vo
l.
44
, N
o.
5
Bro
wn
pa
pe
r /
pla
stic
Am
bie
nt
Te
mp
era
ture
Re
fer
to
Six
tee
nth
Sch
ed
ule
(Re
gu
latio
n
41
)
Organochlorine S.Pyrethroid
Fre
sh
Fru
its &
Ve
ge
tab
les
1 k
g
Carbamate
F0
4-0
01
Mu
ltip
le
Sim
ulta
ne
ou
s
Me
tho
d f
or
Pe
sticid
e
Re
sid
ue
s in
Fru
its
an
d V
eg
eta
ble
s
DO
C.
NO
TE
ST
ME
TH
OD
GROUPR
EF
ER
EN
CE
PA
RA
ME
TE
RF
OO
DM
AT
RIX
MIN
IMU
M
WE
IGH
TL
OQ
(m
g/k
g)
C
ON
TA
INE
RT
RA
NS
PO
RT
AT
ION
ST
OR
AG
E
MA
XIM
UM
RE
SID
UE
LIM
ITS
(MR
Ls)
in f
oo
d
(mg
/kg
)
MKAK
MKA IPOH
MKA JB
MKA KK
KUCHING
KEDAH
PERLIS
PULAU PINANG
SELANGOR
PAHANG
KELANTAN
TERENGGANU
16
Azin
ph
os e
thyl
0.0
25
Ca
rbo
fen
oth
ion
0.1
Ch
lorp
yri
ph
os
0.0
25
Ch
lorp
yrifo
s m
eth
yl
0.0
25
Cya
no
fen
ph
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gu
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No
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Re
fer
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Six
tee
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gu
latio
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41
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ME
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C.
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De
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Dia
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35
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eth
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0.0
11
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36
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De
term
ina
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Org
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Pe
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y G
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rom
ato
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85
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OA
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pe
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Am
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Te
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To
tal C
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Fre
sh
Fru
its &
Ve
ge
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les
1 k
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Re
fer
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Six
tee
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Sch
ed
ule
(Re
gu
latio
n
41
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OrganophosporusCS2
F0
4-0
15
DO
C.
NO
TE
ST
ME
TH
OD
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RE
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RE
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SID
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resid
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osa
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21
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pta
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pta
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18
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n o
f
Ca
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ma
te In
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tho
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an
ua
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Wa
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Alli
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Syste
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Ca
rba
ma
te A
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lysis
Ald
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it a
nd
Ve
ge
tab
les
1 k
g0
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Bro
wn
Pa
pe
r /
Pla
stic
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bie
nt
Te
mp
era
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Me
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ds o
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l C
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Vo
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wn
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ish
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17
De
term
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Org
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lori
ne
Pe
sticid
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ato
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ze
n
Re
fer
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Six
tee
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ed
ule
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gu
latio
n
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TE
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ME
TH
OD
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RE
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RE
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EP
AR
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FO
OD
MA
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MA
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KUCHING
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jad
ua
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resid
u r
ac
un
per
osa
k
22
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ph
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oa
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De
me
ton
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0.0
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De
me
ton
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eth
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0.0
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top
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0.0
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ph
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thyl
0.0
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os
0.0
5
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0.0
5
Azin
ph
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eth
yl
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hos
0.0
5
Alp
ha
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su
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Be
ta-e
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lfa
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eth
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21
De
term
ina
tio
n o
f
Pe
sticid
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tho
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sticid
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tho
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fer
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ed
ule
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gu
latio
n
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urn
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f A
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Jo
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l V
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12
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pe
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stic
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nt
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fer
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gu
latio
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pe
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stic
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bie
nt
Te
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DO
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TE
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OD
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RE
NC
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OD
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ER
TR
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AG
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MA
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UM
RE
SID
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ua
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TE
ST
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RE
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rne
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t
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G0
4-0
02
Qu
alit
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An
aly
sis
of
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So
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RR
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in
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So
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n P
rod
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Te
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or
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y
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com
bin
ant D
NA
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ch
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s;
Pro
vis
ion
al
Tra
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y M
HL
W
Ro
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du
p
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A
G0
4-0
03
Qu
an
tita
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aly
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du
p R
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Usin
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igh
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5
Ma
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A
G0
4-0
04
Th
e D
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So
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05
Th
e D
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f Z
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Ke
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rn P
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Ze
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rn K
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els
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d c
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se
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pro
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Ke
rne
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. 2
kg
Pro
du
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:
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.
20
0g
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0.1
%
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4-0
06
Th
e D
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ctio
n o
f
Pa
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Po
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po
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ba
se
d
pro
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Ra
w :
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. 3
kg
Pro
du
cts
:
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.
20
0g
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ck
No
t
Ava
ilab
le
Te
stin
g f
or
Fo
od
Pro
du
ce
d b
y
Re
com
bin
ant D
NA
Te
ch
niq
ue
s;
Pro
vis
ion
al
Tra
nsla
tio
n b
y M
HL
W
So
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ea
n
ke
rne
ls a
nd
so
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n
ba
se
d
pro
du
cts
Ke
rne
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. 2
kg
Pro
du
cts
:
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acks,
Min
.
20
0g
/pa
ck
An
y s
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ble
co
nta
ine
r o
r
orig
ina
l
pa
cka
gin
g
As p
urc
ha
se
d
24
G0
4-0
08
Scre
en
ing
of
Ge
ne
tica
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od
ifie
d
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od
an
d Its
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du
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MV
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S P
rom
ote
r)
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ce
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com
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ch
niq
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s;
Pro
vis
ion
al
Tra
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tio
n b
y M
HL
W
(b)
MS
ISO
21
56
9:2
00
7
Ge
ne
tica
lly
Mo
difie
d F
oo
dD
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A
G0
4-0
09
Scre
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of
Ge
ne
tica
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od
ifie
d
Fo
od
an
d Its
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s 3
'
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rmin
ato
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ne
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A
G0
4-0
10
Qu
alit
ative
An
aly
sis
of
Ma
ize
Bt
11
in
Corn
Ke
rne
ls a
nd
Co
rn
Pro
du
cts
Ma
ize
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11
De
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n
Co
rn K
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els
an
d c
orn
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se
pro
du
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%
G0
4-0
11
Qu
alit
ative
An
aly
sis
of
Ma
ize
Bt
17
6 in
Corn
Ke
rne
ls a
nd
Co
rn
Pro
du
cts
Ma
ize
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17
6D
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ctio
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G0
4-0
12
Qu
alit
ative
An
aly
sis
of
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ize
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10
in
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rn K
ern
els
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d C
orn
Pro
du
cts
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ize
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N
81
0D
ete
ctio
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G0
4-0
13
Qu
alit
ative
An
aly
sis
of
Ma
ize
GA
21
in
Corn
Ke
rne
ls a
nd
Co
rn
Pro
du
cts
Ma
ize
GA
21
De
tectio
n0
.1%
G0
4-0
14
Qu
alit
ative
An
aly
sis
of
Ne
wL
ea
f P
lus in
Po
tato
an
d P
ota
to
Pro
du
cts
Ne
wL
ea
f P
lus
De
tectio
n
Po
tato
an
d
po
tato
ba
se
pro
du
cts
No
t
Ava
ilab
le
So
yb
ea
n
ke
rne
ls &
so
yb
ea
n
pro
du
cts
, co
rn
ke
rne
ls &
co
rn
pro
du
cts
,
po
tato
&
po
tato
pro
du
cts
Ke
rne
ls/R
aw
:
Min
. 2
kg
Pro
du
cts
:
2 p
acks,
Min
.
20
0g
/pa
ck
Ke
rne
ls :
Min
. 2
kg
Pro
du
cts
:
2 p
ack,
Min
.
20
0g
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ck
Te
stin
g f
or
Fo
od
Pro
du
ce
d b
y
Re
com
bin
ant D
NA
Te
ch
niq
ue
s;
Pro
vis
ion
al
Tra
nsla
tio
n b
y M
HL
W
An
y s
uita
ble
co
nta
ine
r o
ro
rig
ina
l
pa
cka
gin
g
As p
urc
ha
se
d
Co
rn K
ern
els
an
d c
orn
ba
se
pro
du
cts
DO
C.
NO
TE
ST
ME
TH
OD
RE
FE
RE
NC
EP
AR
AM
ET
ER
ME
TH
OD
FO
OD
MA
TR
IXM
INIM
UM
WE
IGH
TL
OQ
CO
NT
AIN
ER
TR
AN
SP
OR
TA
TIO
N
ST
OR
AG
E
MKAK
MKA IPOH
MKA JB
MKA KK
KUCHING
KEDAH
PERLIS
PULAU PINANG
SELANGOR
PAHANG
KELANTAN
TERENGGANU
Raw
:
Min
. 3 k
g
Pro
ducts
:
2 p
acks,
Min
. 200g/p
ack
Ke
rne
ls:
Min
. 2
kg
Pro
du
cts
:
2 p
ack,
Min
.
20
0g
/pa
ck
jad
ua
l 1
.4
bio
tek
no
lo
gi
ma
ka
na
n
25
G0
4-0
15
Qu
alit
ative
An
aly
sis
of
Ne
wL
ea
fY
in
Po
tato
an
d P
ota
to P
rod
ucts
Te
stin
g f
or
Fo
od
Pro
du
ce
d b
y
Re
co
mb
ina
nt
DN
A
Te
ch
niq
ue
s;
Pro
vis
ion
al
Tra
nsla
tio
n b
y M
HL
W
Ne
wL
ea
f Y
De
tectio
n
G0
4-0
18
De
tectio
n o
f A
via
n D
NA
in A
nim
al T
issu
e/M
ea
t
Pro
du
cts
by U
sin
g
TE
PN
EL
Bio
kits
Avia
nD
ete
ctio
n
G0
4-0
19
De
tectio
n o
f B
ovin
e
DN
A in
An
ima
l
Tis
su
e/M
ea
t P
rod
ucts
by U
sin
g T
EP
NE
L
Bio
kits
Bo
vin
eD
ete
ctio
n
G0
4-0
20
De
tectio
n o
f P
orc
ine
DN
A in
An
ima
l
Tis
su
e/M
ea
t P
rod
ucts
by U
sin
g T
EP
NE
L
Bio
kits
Po
rcin
eD
ete
ctio
n
G0
4-0
21
DN
A E
xtr
actio
n U
sin
g
QIA
GE
N D
Ne
asy®
Tis
su
e K
it
QIA
GE
N D
Ne
asy®
Tis
su
e K
it D
Ne
asy®
Tis
su
e H
an
db
oo
k
Extr
actio
n
tissu
e/m
ea
t
No
t
Ap
plic
ab
le
G0
4-0
22
DN
A E
xtr
actio
n U
sin
g
HK
DN
A C
hip
s L
iqu
id
Fo
od
s K
it
Use
r M
an
ua
lfo
r th
e
Exra
ctio
n o
f D
NA
fro
m L
iqu
id
Fo
od
s
Extr
actio
n liq
uid
foo
d
No
t
Ap
plic
ab
le
So
yb
ea
n &
co
rn b
ase
d
pro
du
cts
G0
4-0
23
De
tectio
n o
f P
orc
ine
DN
Au
sin
g R
ea
l T
ime
PC
R
Qu
an
tiF
ast™
SY
BR
®
Gre
en
PC
R
Ha
nd
bo
ok
Po
rcin
eD
ete
ctio
n
An
ima
l tissu
e,
foo
d p
rod
ucts
,
milk
& m
ilk
pro
du
cts
an
d
ed
ible
fat
2 p
acks,
Min
.
20
0g
/pa
ck
An
ima
l tissu
e
an
d f
oo
d
pro
du
cts
Anim
al T
issue:
1 k
g F
oo
d
Pro
du
cts
:
25
0g
Anim
al T
issue:
1 k
g F
oo
d
Pro
du
cts
:
25
0g
Anim
al T
issue:
1 k
g F
oo
d
Pro
du
cts
:
25
0g
or
Bio
kits A
nim
al
Sp
ecia
tio
n M
od
ule
for
PC
R S
cre
en
ing
of
Ra
wa
nd
Pro
ce
ssd
Fo
od
an
d F
ee
d
Pro
du
cts
fo
r th
e
pre
se
nce
of
An
ima
l
Sp
ecie
s
No
t
Ava
ilab
le
An
y s
uita
ble
co
nta
ine
r o
r
orig
ina
l
pa
cka
gin
g
As p
urc
ha
se
d
DO
C.
NO
TE
ST
ME
TH
OD
RE
FE
RE
NC
EP
AR
AM
ET
ER
ME
TH
OD
FO
OD
MA
TR
IXM
INIM
UM
WE
IGH
TL
OQ
CO
NT
AIN
ER
TR
AN
SP
OR
TA
TIO
N
ST
OR
AG
E
MKAK
MKA IPOH
MKA JB
MKA KK
KUCHING
KEDAH
PERLIS
PULAU PINANG
SELANGOR
PAHANG
KELANTAN
TERENGGANU
jad
ua
l 1
.4
bio
tek
no
lo
gi
ma
ka
na
n
26
G0
4-0
24
Qu
alit
ative
An
aly
sis
of
Ma
ize
T2
5 in
Corn
Ke
rne
ls a
nd
Co
rn
Pro
du
cts
Te
stin
gfo
r F
oo
d
Pro
du
ce
d b
y
Re
co
mb
ina
nt
DN
A
Te
ch
niq
ue
s;
Pro
vis
ion
al
Tra
nsla
tio
n b
y M
HL
W
Ma
ize
T2
5D
ete
ctio
n
Co
rn K
ern
els
an
d c
orn
ba
se
pro
du
cts
Ke
rne
ls :
Min
. 2
kg
Pro
du
cts
:
2 p
ack,
Min
.
20
0g
/pa
ck
0.1
%
G0
4-0
25
De
tectio
n o
f B
ub
alu
s
bu
ba
lis D
NA
in
An
ima
l
Tis
su
e/M
ea
t P
rod
ucts
Bio
kits A
nim
al
Sp
ecia
tio
n M
od
ule
fo
PC
R S
cre
en
ing
of
Ra
wa
nd
Pro
ce
ssd
Fo
od
an
d F
ee
d
Pro
du
cts
fo
r th
e
pre
se
nce
of
An
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l
Sp
ecie
s a
nd
Jo
urn
al
of
Da
iry R
ese
arc
h
(20
01
) 6
8 U
se
of
Du
ple
x-P
CR
Te
ch
niq
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to
Id
en
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Bo
vin
e a
nd
Wa
ter
Bu
ffa
lo M
ilku
se
d in
Ma
kin
g M
ozza
rella
Ch
ee
se
Bu
ba
lus b
ub
alis
De
tectio
n
An
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l tissu
e
an
d f
oo
d
pro
du
cts
Anim
al T
issue:
1 k
g F
ood
Pro
ducts
: 250g
G0
4-0
26
DN
A E
xtr
actio
n f
rom
Ed
ible
Fa
t u
sin
g
Ep
ice
ntr
e K
it
Use
rM
an
ua
l fo
r th
e
Exra
ctio
n o
f D
NA
fro
m
Fo
od
s
Extr
actio
n m
ilk
& m
ilkp
rod
ucts
an
d e
dib
le f
at
No
t
Ap
plic
ab
le
Milk
& m
ilk
pro
du
cts
an
d
ed
ible
fa
t
Pro
du
cts
:
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acks,
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.
20
0g
/pa
ck
No
t
Ava
ilab
le
An
y s
uita
ble
co
nta
ine
r o
r
orig
ina
l
pa
cka
gin
g
As p
urc
ha
se
d
DO
C.
NO
TE
ST
ME
TH
OD
RE
FE
RE
NC
EP
AR
AM
ET
ER
ME
TH
OD
FO
OD
MA
TR
IXM
INIM
UM
WE
IGH
TL
OQ
CO
NT
AIN
ER
TR
AN
SP
OR
TA
TIO
N
ST
OR
AG
E
MKAK
MKA IPOH
MKA JB
MKA KK
KUCHING
KEDAH
PERLIS
PULAU PINANG
SELANGOR
PAHANG
KELANTAN
TERENGGANU
jad
ua
l 1
.4
bio
tek
no
lo
gi
ma
ka
na
n
27
jad
ua
l 1
.5
cem
ar
an
lo
ga
m b
er
at
DO
C.
NO
TE
ST
ME
TH
OD
P
AR
AM
ET
ER
PA
RA
ME
TE
RF
OO
D
MA
TR
IX
MIN
IMU
M
WE
IGH
T
LO
Q
(mg
/kg
)
CO
NT
AIN
ER
TR
AN
SP
OR
TA
TIO
N
ST
OR
AG
E
MA
XIM
UM
PE
RM
ITT
ED
PR
OP
OR
TIO
N
(mg
/kg
)
MKAK
MKA IPOH
MKA JB
MKA KK
KUCHING
KEDAH
PERLIS
PULAU PINANG
SELANGOR
PAHANG
KELANTAN
TERENGGANU
H0
4-0
01
Th
e D
ete
rmin
atio
n o
f
Me
rcu
ry in
Fo
od
by
Ato
mic
Ab
so
rptio
n
Sp
ectr
om
ete
r -
Flo
w
Inje
ctio
n A
na
lysis
Syste
m (
AA
S-F
IAS
)
MS
95
4 :
Pa
rt 1
3,
19
89
To
talM
erc
ury
Fis
h a
nd
fish
pro
du
ct
/ sh
ellf
ish
1 k
g
(with
sh
ell)
0.0
7
Pre
da
tory
: 1
,
Oth
er
Fis
h :
0.5
,
Oth
er
Fo
od
Ma
tric
es :
0.0
5
AF
AF
Plu
mb
um
0.7
50
.1 -
2*
AF
Ca
dm
ium
0.0
71
AF
AF
To
tal A
rse
nic
10
.1 -
1*
Sta
nu
m1
0
Pa
cke
d w
ith
ca
n o
r tin
fo
il:
25
0,
Oth
ers
:4
0A
F
Plu
mb
um
0.0
40
.1 -
2*
AA
F
Ars
en
ic0
.20
.1 -
1*
Ca
dm
ium
0.1
1
Plu
mb
um
0.7
50
.2 -
2*
A
Ca
dm
ium
0.2
51
AF
AA
H0
4-0
05
Th
e D
ete
rmin
atio
n o
f
Me
rcu
ry in
Fo
od
by
Ato
mic
Ab
so
rptio
n
Sp
ectr
op
ho
tom
etr
y
(AA
S)
Co
ld V
ap
ou
r
Acce
sso
rie
s (
AV
A)
Fo
od
Qu
alit
y C
on
tro
l
Div
isio
n,
19
97
. T
he
De
term
ina
tio
n o
f
Me
rcu
ry in
Fo
od
an
d
Blo
od
by A
tom
ic
Sp
ectr
om
etr
y (
AA
S)
usin
g a
n A
tom
ic V
ap
or
Acce
sso
ry.
Me
tho
d
5.3
.2
To
talM
erc
ury
Fis
h a
nd
fish
pro
du
ct
/ sh
ellf
ish
1 k
g (
with
sh
ell)
0.0
3
Pre
da
tory
: 1
,
Oth
er
Fis
h :
0.5
,
Oth
er
Fo
od
Ma
tric
es :
0.0
5
AF
H0
4-0
03
H0
4-0
04
50
0 g
/ml
50
0 g
/ml
Th
e D
ete
rmin
atio
n o
f
Plu
mb
um
, C
ad
miu
m a
nd
Ars
en
ic in
Fo
od
by
Gra
ph
ite
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4-0
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4-0
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11
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era
tio
n o
f L
iste
ria
Mo
no
cyto
ge
ne
sL
iste
ria
mo
no
cyto
ge
ne
sE
nu
me
ratio
n1
00
CF
U/g
K0
4-0
10
-04
Exa
min
atio
n f
or
Vib
rio
Pa
rah
ae
mo
lyticu
sV
ibrio
pa
rah
ae
mo
lyticu
sD
ete
ctio
nL
OD
: 0
.04
cfu
/gA
AA
K0
4-0
05
-01
Th
e E
nu
me
ratio
n o
f C
oa
gu
lase
Po
sitiv
e
Sta
ph
ylo
co
cci-T
ech
niq
ue
usin
g B
aird
-Pa
rke
r
Ag
ar
Me
diu
m
Co
ag
ula
se
Po
sitiv
e
Sta
ph
ylo
co
cci
De
tectio
nL
OD
: 0
.04
cfu
/gA
K0
4-0
02
-05
Ye
ast
an
d M
ou
ld C
ou
nt
in F
oo
d-
Co
mp
act
Dry
Nis
su
iY
ea
st
& m
ou
ldE
nu
me
ratio
n1
00
CF
U/g
DO
C.N
OT
ES
TM
ET
HO
DP
AR
AM
ET
ER
TE
CH
NIQ
UE
LO
Q
MKAK
MKA IPOH
MKA JB
MKA KK
KUCHING
PERLIS
P. PINANG
SELANGOR
PAHANG
KELANTAN
TERENGGANU
SANDAKAN
MIRI
En
um
era
tio
n o
f L
actic A
cid
Ba
cte
ria
-Co
lon
y
Co
un
t T
ech
niq
ue
at
30
C
o
jad
ua
l 1
.7
mik
ro
bio
lo
gi
ma
ka
na
n
34
jad
ua
l 1
.8 c
em
ar
an
mik
olo
gi
DO
C.
NO
TE
ST
ME
TH
OD
PA
RA
ME
TE
RP
AR
AM
ET
ER
FO
OD
MA
TR
IX
MIN
IMU
M
WE
IGH
T
LO
D
(µg/k
g)
CO
NT
AIN
ER
TR
AN
SP
OR
TA
TIO
N
ST
OR
AG
E
MA
XIM
UM
PE
RM
ITT
ED
PR
OP
OR
TIO
N
(µg
/kg
)
MKAK
MKA IPOH
MKA JB
MKA KK
KUCHING
KEDAH
PERLIS
PULAU PINANG
SELANGOR
PAHANG
KELANTAN
TERENGGANU
Afla
toxin
s B
12
.5
Afla
toxin
s B
21
.2
Afla
toxin
s G
13
.2
Afla
toxin
s G
21
.2
Afla
toxin
s B
10
.8
Afla
toxin
s B
20
.4
Afla
toxin
s G
10
.8
Afla
toxin
s G
20
.4
L0
4-0
05
De
term
ina
tio
n o
f
Och
rato
xin
A in
Ric
e a
nd
Wh
ea
t b
y u
sin
g
Imm
un
oa
ffin
ity C
olu
mn
Cle
an
Up
Me
tho
d
VIC
AM
Och
raT
est
Instr
uctio
nM
an
ua
l
Me
tho
d N
um
be
r 5
.8
Och
rato
xin
A
Ric
e,
Wh
ea
t
Flo
ur
&
Co
co
a
Po
wd
er
1 k
g2
.55
A
L0
4-0
06
De
term
ina
tio
n o
f
Och
rato
xin
A in
Co
ffe
e
by u
sin
g Im
mu
no
aff
inity
Co
lum
n C
lea
n U
p
Me
tho
d
VIC
AM
Och
raT
est
Instr
uctio
nM
an
ua
l
Me
tho
d N
um
be
r 5
.4
Och
rato
xin
AC
off
ee
1
kg
0.5
5A
L0
4-0
07
Qu
an
tita
tive
An
aly
sis
fo
r
Fe
ed
an
d C
ere
al b
y
usin
g R
ida
scre
en
Fa
st
Afla
toxin
Kit In
str
uctio
nM
an
ua
lA
fla
toxin
Ce
rea
l1
kg
1
.755
L0
4-0
03
Ch
illie
sa
nd
chill
i
pro
du
cts
Th
e D
ete
rmin
atio
n o
f
Afla
toxin
s B
1,
B2
, G
1
an
d G
2 in
Drie
d C
hill
ies
by U
sin
g
Imm
un
oa
ffin
ity C
olu
mn
Cle
an
Up
Me
tho
d
5
Pro
ce
sse
d
foo
d :
5
Ra
w
pe
an
uts
: 1
5
Ro
om
Te
mp
era
ture
5A
AA
Pe
an
uts
an
d r
ice
With
ou
t
sh
ell
:
1 k
g
With
sh
ell
:1.5
kg
Th
e D
ete
rmin
atio
n o
f
Afla
toxin
s B
1,
B2
, G
1
an
d G
2 in
Pe
an
uts
an
d
Ric
e b
y U
sin
g
Mu
ltifu
nctio
na
l C
olu
mn
Cle
an
Up
Me
tho
d
L0
4-0
02
AO
AC
99
4.0
8,
20
00
L0
4-0
04
De
term
ina
tio
n o
f
Ze
ara
len
on
e in
Ric
e a
nd
Wh
ea
t F
lou
r b
y u
sin
g
Imm
un
oa
ffin
ity C
olu
mn
Cle
an
Up
Me
tho
d
1 k
g
VIC
AM
Afla
Te
st
Instr
uctio
nM
an
ua
l
Me
tho
d N
um
be
r 5
.10
an
d 5
.13
Ric
e a
nd
Wh
ea
t
Flo
ur
1 k
g
VIC
AM
Ze
ara
laT
est
Instr
uctio
nM
an
ua
l
Me
tho
d N
um
be
r 5
.3O
rig
ina
l
Pa
cka
gin
g /
Pla
stic /
Pa
per
Ze
ara
len
on
e
35
jad
ua
l 1
.8 c
em
ar
an
mik
olo
gi
L0
4-0
08
Qu
an
tita
tive
An
aly
sis
fo
r
Fe
ed
an
d C
ere
al b
y
usin
g R
ida
scre
en
Fa
st
Ze
ara
len
on
e
Kit In
str
uctio
nM
an
ua
lZ
ea
rale
no
ne
Fe
ed
an
d
Ce
rea
l1
kg
50
5
L0
4-0
09
Qu
an
tita
tive
An
aly
sis
fo
r
Fe
ed
an
d C
ere
al b
y
usin
g R
ida
scre
en
Fa
st
Och
rato
xin
A
Kit In
str
uctio
nM
an
ua
lO
ch
rato
xin
AF
ee
d a
nd
Ce
rea
l1
kg
55
Afla
toxin
B1
0.4
Afla
toxin
B2
0.2
Afla
toxin
G1
0.4
Afla
toxin
G2
0.2
Afla
toxin
s B
10
.4
Afla
toxin
s B
20
.2
Afla
toxin
s G
10
.4
Afla
toxin
s G
2
0.2
L0
4-0
13
De
term
ina
tio
n o
f
Afla
toxin
M1
in M
ilkb
y
usin
g Im
mu
no
aff
inity
Co
lum
n C
lea
n a
nd
HP
LC
Me
tho
d
VIC
AM
Afla
Te
st
Instr
uctio
n M
an
ua
l
Me
tho
d N
um
be
r 5
.6
Afla
toxin
M1
Milk
1kg
0.0
5
Ori
gin
al
Pa
cka
gin
g /
Am
be
r G
lass
Bo
ttle
<4°C
for
pa
ste
urise
d m
ilk
(ch
ill)
/ R
oo
m
Te
mp
era
ture
fo
r
UH
Ta
nd
Ste
riliz
ed
Milk
0.5
Afla
toxin
B1
0.8
Afla
toxin
B2
0.4
Afla
toxin
G1
0.8
Afla
toxin
G2
0.4
AA
5
L0
4-0
14
De
term
ina
tio
n o
f
Afla
toxin
B1
, B
2,
G1
an
d
G2
in
Nu
ts,
Ce
rea
l a
nd
Fis
h b
y u
sin
g
Imm
un
oa
ffin
ity C
olu
mn
Cle
an
Up
Me
tho
d a
nd
HP
LC
With
PH
RE
D
Me
tho
d
Pe
an
uts
,
Tre
en
uts
(e.g
alm
on
d,
ha
ze
l &
pis
tach
io),
Ce
rea
l &
Fis
h
Pro
du
cts
De
term
ina
tio
n o
f
Afla
toxin
s B
1,
B2
, G
1
an
d G
2 in
Ric
e b
y U
sin
g
Imm
un
oa
ffin
ity C
olu
mn
Cle
an
Up
Me
tho
d
L0
4-0
11
De
term
ina
tio
n o
f
Afla
toxin
s B
1,
B2
, G
1
an
d G
2 in
Pe
an
uts
by
Usin
g Im
mu
no
aff
inity
Co
lum
n C
lea
n U
p
Me
tho
d
Pro
ce
sse
d
foo
d :
5
Ra
w
pe
an
uts
: 1
5
VIC
AM
Afla
Te
st
Instr
uctio
n M
an
ua
l
Me
tho
d N
um
be
r 5
.3
VIC
AM
Afla
Te
st
Instr
uctio
n M
an
ua
l
Me
tho
d N
um
be
r 5
.4
an
d 5
.12
AO
AC
Off
icia
l M
eth
od
99
1.3
1 a
nd
VIC
AM
Afla
Te
st
Instr
uctio
n
Ma
nu
al M
eth
od
Nu
mb
er
5.4
an
d 5
.12
Pe
an
uts
Ric
e
Ori
gin
al
Pa
cka
gin
g /
Pla
stic /
Pa
pe
r
Ro
om
Te
mp
era
ture
1 k
g
with
ou
t
sh
ell
/
1.5
kg
with
sh
ell
L0
4-0
12
Pro
ce
sse
d
foo
d :
5
Ra
w
pe
an
uts
: 1
5
A
Ro
om
Te
mp
era
ture
1 k
g
1 k
g
with
ou
t
sh
ell
/
1.5
kg
with
sh
ell
Ori
gin
al
Pa
cka
gin
g /
Pla
stic /
Pa
pe
r
DO
C.
NO
TE
ST
ME
TH
OD
PA
RA
ME
TE
RP
AR
AM
ET
ER
FO
OD
MA
TR
IX
MIN
IMU
M
WE
IGH
T
LO
D
(µg/k
g)
CO
NT
AIN
ER
TR
AN
SP
OR
TA
TIO
N
ST
OR
AG
E
MA
XIM
UM
PE
RM
ITT
ED
PR
OP
OR
TIO
N
(µg
/kg
)
MKAK
MKA IPOH
MKA JB
MKA KK
KUCHING
KEDAH
PERLIS
PULAU PINANG
SELANGOR
PAHANG
KELANTAN
TERENGGANU
36
L0
4-0
15
De
term
ina
tio
n o
f
De
oxyn
iva
len
ol in
Ric
e,
Ma
ize
an
d W
he
at
Pro
du
ct
by u
sin
g
Imm
on
ua
ffin
ity c
olu
mn
an
d H
PL
C
VIC
AM
DO
NT
est
HP
LC
Instr
uctio
n
Ma
nu
alM
eth
od
Nu
mb
er
4.1
De
oxyn
iva
len
ol
Ce
rea
ls1
kg
80
Ori
gin
al
Pa
cka
gin
g /
Am
be
r G
lass
Bo
ttle
Ro
om
Te
mp
era
ture
5
L0
4-0
16
Qu
an
tita
tive
An
aly
sis
fo
r
Milk
by R
ida
scre
en
Fa
st
Afla
toxin
M1
Kit In
str
uctio
n M
an
ua
lA
fla
toxin
M1
Milk
50
0 m
l0
.5
Ori
gin
al
Pa
cka
gin
g/
Am
be
r P
lastic
Bo
ttle
< 4
0C
fo
r
pa
ste
urise
d m
ilk
(ch
ill)/
Ro
om
Te
mp
era
ture
fo
r
UH
Ta
nd
Ste
riliz
ed
Milk
0.5
DO
C.
NO
TE
ST
ME
TH
OD
PA
RA
ME
TE
RP
AR
AM
ET
ER
FO
OD
MA
TR
IX
MIN
IMU
M
WE
IGH
T
LO
D
(µg/k
g)
CO
NT
AIN
ER
TR
AN
SP
OR
TA
TIO
N
ST
OR
AG
E
MA
XIM
UM
PE
RM
ITT
ED
PR
OP
OR
TIO
N
(µg
/kg
)
MKAK
MKA IPOH
MKA JB
MKA KK
KUCHING
KEDAH
PERLIS
PULAU PINANG
SELANGOR
PAHANG
KELANTAN
TERENGGANU
jad
ua
l 1
.8 c
em
ar
an
mik
olo
gi
37
jad
ua
l 1
.9 pem
bu
ng
ku
sa
n
DO
C.
NO
TE
ST
ME
TH
OD
STATUSR
EF
ER
EN
CE
PA
RA
ME
TE
RF
OO
DM
AT
RIX
MIN
IMU
M W
EIG
HT
LO
Q
(mg/k
g)
CO
NT
AIN
ER
TR
AN
SP
OR
TA
TIO
N
ST
OR
AG
EM
AX
IMU
M P
ER
MIT
TE
D P
RO
PO
RT
ION
Ja
pa
n S
an
ita
tio
n L
aw
, 1
99
9
1.
To
lue
ne
●S
tyre
ne
= ≤
10
00
mg
/kg
2.
Eth
ylb
en
ze
ne
●E
thylb
en
ze
ne
= ≤
10
00
mg
/kg
3.
iso
-Pro
pylb
en
ze
ne
●T
ota
l co
nce
ntr
atio
n o
f 5
co
mp
ou
nd
s =
4.
n-P
rop
ylb
en
ze
ne
≤ 5
00
0 m
g/k
g
5.
Sty
ren
e
≤ 2
00
0 m
g/k
g (
PS
fo
am
)
≤ 1
50
0 m
g/k
g
(m
ilk &
milk
pd
t)
1.
Ph
en
ol
Ja
pa
n S
an
ita
tio
n L
aw
, 1
99
9
2.
Bis
ph
en
ol A
Ma
teri
al T
est
3.
p-t
Bu
tylp
he
no
l●
Dip
he
nylc
arb
on
te =
≤ 5
00
mg
/kg
4.
Dip
he
nylc
arb
on
ate
●T
ota
l co
nce
ntr
atio
n o
f 3
co
mp
ou
nd
s (
Bis
ph
en
ol A
, P
he
no
l,
p-t
bu
tylp
he
no
l) =
≤ 5
00
mg
/kg
1.
Ph
en
ol
Ja
pa
n S
an
ita
tio
n L
aw
, 1
99
9
2.
Bis
ph
en
ol A
Mig
ratio
n T
est
3.
p-t
Bu
tylp
he
no
lB
isp
he
no
l A
= ≤
2.5
mg
/kg
4.
Dip
he
nylc
arb
on
ate
Sp
ecific
atio
n a
nd
Sta
nd
ard
sfo
r fo
od
s,
the
ir
co
nta
ine
rs a
nd
pa
cka
ge
s
etc
.
(B
ase
d o
n t
he
Fo
od
Sa
nita
tio
n L
aw
),
Ja
pa
n F
oo
d H
yg
ien
e
Asso
cia
tio
n,
19
92
Sp
ecific
atio
n a
nd
Sta
nd
ard
sfo
r fo
od
s,
the
ir
co
nta
ine
rs a
nd
pa
cka
ge
s
etc
.
(B
ase
d o
n t
he
Fo
od
Sa
nita
tio
n L
aw
),
Ja
pa
n F
oo
d H
yg
ien
e
Asso
cia
tio
n,
19
92
● p
acka
ge
with
ou
t fo
od
-
orig
ina
l
co
nta
ine
r /
wra
pp
ed
with
pa
pe
r /
Alu
min
ium
/
hig
h r
esis
tan
t
pla
stic
Ro
om
Te
mp
era
ture
/
Sa
me
Te
mp
era
ture
co
nd
itio
n w
he
n it
is
sam
ple
d
Ro
om
Te
mp
era
ture
/
Sa
me
Te
mp
era
ture
co
nd
itio
n w
he
n it
is
sam
ple
d
MO
H
M0
4-0
03
De
term
ina
tio
n o
f
Bis
ph
en
ol A
, P
he
no
l, p
-t
Bu
thylp
he
no
l a
nd
Dip
he
nylc
arb
on
ate
in
Fo
od
Co
nta
ct
Ma
teri
als
usin
g H
igh
Pe
rfo
rma
nce
Liq
uid
Ch
rom
ato
gra
ph
y
(Mig
ratio
n T
est)
Po
lyca
rbo
na
te
(PC
)
1.
Co
nta
ine
r :
≥ 4
un
its
● p
acka
ge
co
nta
inin
g
foo
d in
co
nta
ct
-
orig
ina
l
co
nta
ine
r
8m
g/k
g
Po
lysty
ren
e
(PS
)
Po
lyca
rbo
na
te
(PC
)
1.
Stirr
er/
sp
oo
n/
fork
/ ch
op
stick :
≥ 5
un
its
2.
Co
nta
ine
r/
pla
tes/
cu
ps/
tra
y :
≥ 2
un
its
1.
Co
nta
ine
r :
≥ 1
un
it
0.5
mg/L
(Phenol, p
-t-
buty
lphenol,
dip
henylc
arb
onate
)
MO
H
M0
4-0
01
10
mg
/kg
3.
Oth
ers
:
≥ 2
un
its
De
term
ina
tio
n o
f
Re
sid
ua
l S
tyre
ne
Mo
no
me
r a
nd
Oth
er
Vo
latile
Org
an
ic
Co
mp
ou
nd
s (
VO
Cs)
in
Fo
od
Co
nta
ct
Ma
teri
als
usin
g G
as
Ch
rom
ato
gra
ph
y
MO
H
M0
4-0
02
De
term
ina
tio
n o
f re
sid
ua
l
Bis
ph
en
ol A
, P
he
no
l, p
-t
Bu
thylp
he
no
l a
nd
Dip
he
nylc
arb
on
ate
in
Fo
od
Sim
ula
nts
usin
g
Hig
h P
erf
orm
an
ce
Liq
uid
Ch
rom
ato
gra
ph
y
(Ma
teria
ln T
est)
Th
e P
ha
rma
ce
utica
l
So
cie
ty o
f Ja
pa
n
(Hyg
ien
e T
est
Me
tho
d
No
te)
A
0.2
mg
/L
(Bis
ph
en
ol A
)
PS6
OT
HE
R
7
OT
HE
R
7
38
1. D
ieth
yl phath
ala
te (
DE
P)
Po
lysty
ren
e (
PS
)
2. D
i-is
o-p
ropyl phth
ala
te (
DiP
P)
3. D
i-n-p
ropyl phth
ala
te (
DnP
P)
4. D
i-is
o b
uty
l phth
ala
te (
DiB
P)
5. D
i-n-b
uty
l sebacate
(D
BS
)
6. B
uty
l phth
aly
buty
l gly
cola
te
(BP
BG
)
7. D
i-hexyl phth
ala
te (
DH
xP
)
8. D
i-cylo
hexyl phth
ala
te
(DC
HP
)
9. T
ri-n
-buty
l tr
imery
tate
(T
BT
M)
Po
lycarb
on
ate
(P
C)
10. D
i-2-e
thylh
exyl azela
te
(DE
HA
8)
Conta
iner
: 1 u
nit
11. D
imeth
yl phth
ala
te (
DM
P)
12. D
i-n-b
uty
l phth
ala
te (
DnB
P)
Po
lyvin
yl ch
lori
de
(PV
C)
13. D
ipenty
l phth
ala
te (
DP
eP
)&
14. A
cety
l-tr
i-n-b
uty
l citra
te
(AT
BC
)
15. B
uty
l benzyl phth
ala
te (
BB
P)
16. D
i-2-e
thyl hexyl adip
ate
(DE
HA
)C
onta
iner
: 1 u
nit
17. T
ri-2-e
thyl
hexy
l phth
ala
te (T
OP
)
18. D
i-2-e
thylh
exyl phth
ala
te
(DE
HP
)
19. D
i-n-o
cty
l phth
ala
te (
DnO
P)
20. T
ri-2
-eth
ylh
exyl tr
imelli
tate
(TO
TM
)
21. D
i-hepty
l phth
ala
te (
DhpP
)
22. D
i-is
o-n
onyl phth
ala
te (
DIN
P)
AM
OH
M04-
004
Dete
rmin
ation o
f
Pla
sticiz
ers
in F
ood
Conta
ct M
ate
rial usin
g
Gas C
hro
mato
gra
ph
● p
ackage
conta
inin
g
food in
conta
ct -
origin
al
conta
iner
● p
ackage
without fo
od -
origin
al
conta
iner
/
wra
pped w
ith
paper
/
Alu
min
ium
/
hig
h r
esis
tant
pla
stic
Room
Tem
pera
ture
/
sam
e tem
pera
ture
conditio
n w
hen it is
sam
ple
d
Poly
styr
ene (P
S)
Poly
vin
yl
chlo
ride (
PV
C)/
Maste
r T
hesis
of Z
alil
ah
Nasir
2.
Conta
iner/
pla
tes/
cups/ tr
ay :
≥ 2
units
1.
Stirr
er/
spoon/
fork
/ chopstick :
≥ 5
units
3.
Oth
ers
:
≥ 2
units
Poly
carb
onate
(PC
)
40m
g/k
g
Po
lyvin
ylid
ine
Ch
lori
de (
PV
DC
)
Poly
vin
ylid
ine
Chlo
ride (P
VD
C)
Japan S
anitation L
aw
,Code o
f
Federa
l R
egula
tions ,
US
AE
uro
pean L
egis
lation,
EU
(Types o
f banned p
lasticiz
ers
)
DO
C.
NO
TE
ST
ME
TH
OD
STATUS
RE
FE
RE
NC
EP
AR
AM
ET
ER
FO
OD
MA
TR
IXM
INIM
UM
WE
IGH
TL
OQ
(mg/k
g)
CO
NT
AIN
ER
TR
AN
SP
OR
TA
TIO
N
ST
OR
AG
EM
AX
IMU
M P
ER
MIT
TE
D P
RO
PO
RT
ION
PV
C3
jad
ua
l 1
.9 pem
bu
ng
ku
sa
n
39
2
DO
C.
NO
TE
ST
ME
TH
OD
STATUS
RE
FE
RE
NC
EP
AR
AM
ET
ER
FO
OD
MA
TR
IXM
INIM
UM
WE
IGH
TL
OQ
CO
NT
AIN
ER
TR
AN
SP
OR
TA
TIO
N
ST
OR
AG
EM
AX
IMU
M P
ER
MIT
TE
D P
RO
PO
RT
ION
jad
ua
l 1
.9 pem
bu
ng
ku
sa
n
40
µ
≥
DO
C.
NO
TE
ST
ME
TH
OD
STATUS
RE
FE
RE
NC
EP
AR
AM
ET
ER
FO
OD
MA
TR
IXM
INIM
UM
WE
IGH
TL
OQ
C
ON
TA
INE
RT
RA
NS
PO
RT
AT
ION
ST
OR
AG
EM
AX
IMU
M P
ER
MIT
TE
D P
RO
PO
RT
ION
jad
ua
l 1
.9 pem
bu
ng
ku
sa
n
41
DO
C.
NO
TE
ST
ME
TH
OD
RE
FE
RE
NC
EP
AR
AM
ET
ER
FO
OD
MA
TR
IX
MIN
IMU
M
WE
IGH
T
LO
Q
(mg/k
g)
C
ON
TA
INE
RT
RA
NS
PO
RT
AT
ION
ST
OR
AG
E
RE
GU
LA
TO
RY
LIM
IT
MKAK
MKA IPOH
MKA JB
MKA KK
KUCHING
KEDAH
PERLIS
PULAU PINANG
SELANGOR
PAHANG
KELANTAN
TERENGGANU
Nitrite
Nitra
te
Ch
lorid
e
Bro
mid
e
N0
4-0
03
Th
e D
ete
ctio
n o
f P
ea
nu
t
Alle
rge
n in
Fo
od
by
usin
g A
lert
® P
ea
nu
t
Alle
rge
n S
cre
en
ing
Te
st
Kit In
str
uctio
n M
an
ua
lP
ea
nu
t
Alle
rgen
Pe
an
ut
pro
du
cts
5
N0
4-0
04
Th
e D
ete
rmin
atio
n o
f
Pe
an
ut
Alle
rge
n In
Fo
od
By U
sin
g V
era
tox®
Qu
an
tita
tive
Pe
an
ut
Alle
rge
nT
est
Kit In
str
uctio
n M
an
ua
lP
ea
nu
t
Alle
rgen
Pe
an
ut
pro
du
cts
2.5
N0
4-0
05
Th
e D
ete
ctio
n o
f M
ilk
Alle
rge
n In
Fo
od
Usin
g
Ale
rt®
Milk
Alle
rge
n
Scre
en
ing
Te
st
Kit In
str
uctio
n M
an
ua
lM
ilk A
llerg
en
Milk
pro
du
cts
5
N0
4-0
06
Th
e D
ete
rmin
atio
n o
f
Milk
Alle
rge
n In
Fo
od
Usin
g V
era
tox®
To
tal
Milk
alle
rge
n
Qu
an
tita
tive
Te
st
Kit
Kit In
str
uctio
n M
an
ua
lM
ilk A
llerg
en
Milk
pro
du
cts
2.5
N0
4-0
07
Th
e D
ete
ctio
n o
f E
gg
Alle
rge
n In
Fo
od
Usin
g
Ale
rt® E
gg
Alle
rge
n
Scre
en
ing
Te
st
Kit In
str
uctio
n M
an
ua
lE
gg
Alle
rge
nE
gg
pro
du
cts
5
Ori
gin
al
pa
cka
gin
g5
00
g
5
1 k
g
Ric
e
Ve
ge
tab
les
N0
4-0
02
De
term
ina
tio
n o
f
Ch
lorid
e a
nd
Bro
mid
e in
Ric
e u
sin
g Io
n
Ch
rom
ato
gra
ph
y S
yste
m
US
En
vir
on
me
nta
l
Pro
tectio
n A
ge
ncy
(EP
A M
eth
od
90
56
A
Re
vis
ion
1 F
eb
20
07
)
US
En
vir
on
me
nta
l
Pro
tectio
n A
ge
ncy
(EP
A M
eth
od
90
56
A
Re
vis
ion
1 F
eb
20
07
)
10
Ro
om
Te
mp
era
ture
or
ch
ille
d if
mo
re t
ha
n
24
ho
urs
Ro
om
Te
mp
era
ture
No
Re
gu
latio
n
Re
fer
to F
oo
d
Re
gu
latio
n 1
98
5
Bro
wn
Pa
pe
r
Pla
stic
De
term
ina
tio
n o
f N
itra
te
an
d N
itrite
in
Ve
ge
tab
les
usin
g Io
n
Ch
rom
ato
gra
ph
y S
yste
m
N0
4-0
01
jad
ua
l 1
.10
cem
ar
an
sem
ula
ja
di
42
N0
4-0
08
Th
e D
ete
rmin
atio
n O
f
Eg
g A
llerg
en
In
Fo
od
Usin
g V
era
tox®
Qu
an
tita
tive
Eg
g
Alle
rge
n
Te
st
Kit In
str
uctio
nM
an
ua
lE
gg
Alle
rge
nE
gg
pro
du
cts
2.5
N0
4-0
09
Th
e D
ete
ctio
n O
f
Glia
din
In
Fo
od
Usin
g
Ale
rt®
Glia
din
Scre
en
ing
Te
st
Kit In
str
uctio
nM
an
ua
lG
liad
in
Alle
rge
n
Oa
t, B
arl
ey,
Wh
ea
t &
its
pro
du
cts
10
N0
4-0
10
Th
e D
ete
rmin
atio
n O
f
Glia
din
In
Fo
od
Usin
g
Ve
rato
x®
Qu
an
tita
tive
Glia
din
Te
st
Kit In
str
uctio
nM
an
ua
lG
liad
in
Alle
rge
n
Oa
t, B
arl
ey,
Wh
ea
t &
its
pro
du
cts
5
N0
4-0
11
De
term
ina
tio
n o
f
Bio
ge
nic
Am
ine
s in
Fis
h
an
d F
ish
Pro
du
cts
Usin
g
Hig
h P
erf
orm
an
ce
Liq
uid
Ch
rom
ato
gra
ph
y w
ith
Po
st-
Co
lum
n
De
riva
tiza
tio
n
Liq
uid
Ch
rom
ato
gra
ph
y
De
term
ina
tio
n o
f
His
tam
ine
in
fish
,
Sa
ue
rkra
ut
an
d W
ine
:
Inte
rla
bo
rato
ry S
tud
y,
Jo
urn
al o
f A
OA
C
Inte
rna
tio
na
l V
ol. 8
1,
No
. 5
, 1
99
8
His
tam
ine
Tyra
min
e
Ca
da
rve
rin
e
Fis
h a
nd
Fis
h
Pro
du
cts
1kg
30
Ori
gin
al
pa
cka
gin
g/P
l
astic
Fro
ze
n/
as p
urc
ha
se
dN
ot
Ava
ilab
le
N0
4-0
12
Th
e D
ete
rmin
atio
n o
f
To
tal V
ola
tile
Ba
se
Nitro
ge
n (
TV
B-N
) in
Fis
h
Eu
rop
ea
n
Sta
nd
ard
EN
20
74
/20
05
T
VB
NF
ish
1 k
gN
ot
Ava
ilab
le
Pla
stic /
Ori
gin
al
Pa
cka
gin
g
Fro
ze
nN
ot
Ava
ilab
le
N0
4-0
14
Th
e D
ete
rmin
atio
n o
f
Bio
ge
nic
Am
ine
s In
Fo
od
Usin
g H
igh
Pe
rfo
rma
nce
Liq
uid
Ch
rom
ato
gra
ph
y (
HP
LC
)
Jo
urn
al o
f
Ch
rom
ato
gra
ph
y B
, 6
93
(19
97
)
Bio
ge
nic
Am
ine
s
Fis
h a
nd
Fis
h
Pro
du
cts
,
Se
afo
od
an
d
Fe
rme
nte
d
Fo
od
1kg
(w
ith
sh
ell)
10
Pla
stic/
orig
ina
l
pa
cka
gin
g
Ch
illa
nd
fro
ze
n
co
nd
itio
n t
ran
sp
ort
ed
with
in 2
4 h
ou
rs
No
Re
gu
latio
n
Re
fer
to F
oo
d
Re
gu
latio
n 1
98
55
00
g
Ori
gin
al
pa
cka
gin
g
Ro
om
Te
mp
era
ture
DO
C.
NO
TE
ST
ME
TH
OD
RE
FE
RE
NC
EP
AR
AM
ET
ER
FO
OD
MA
TR
IX
MIN
IMU
M
WE
IGH
T
LO
Q
(mg/k
g)
C
ON
TA
INE
RT
RA
NS
PO
RT
AT
ION
ST
OR
AG
E
RE
GU
LA
TO
RY
LIM
IT
MKAK
MKA IPOH
MKA JB
MKA KK
KUCHING
KEDAH
PERLIS
PULAU PINANG
SELANGOR
PAHANG
KELANTAN
TERENGGANU
jad
ua
l 1
.10
cem
ar
an
sem
ula
ja
di
43
ja
du
al 1
.11 k
rit
er
ia p
en
er
ima
an
sa
mpel m
ikr
obio
lo
gi
0-
4.4
°C
–18
°Cto
0°C
Min
imu
m2
50
g o
r
3 p
acks
Sa
mp
les o
f S
he
lfS
tab
le
Pa
cka
ge
d P
rod
ucts
& D
rie
d
Pro
du
cts
TE
MP
ER
AT
UR
E
Sa
mp
le in f
roze
n c
on
ditio
n
Re
fere
nce
Sa
mp
les m
ust
be
inclu
de
d in
th
e ice
bo
x
Ste
rile
Pa
cka
gin
g/
Orig
ina
l P
acka
gin
g
OT
HE
RIN
FO
RM
AT
ION
Ste
rile
Pa
cka
gin
g/
Orig
ina
l P
acka
gin
g2
50
g
Pro
tecte
dfr
om
dir
ect
su
nlig
ht
or
fro
m o
the
r so
urc
es o
f h
ea
t
TY
PE
S O
F S
AM
PL
ES
/
PA
RA
ME
TE
RS
Sa
mp
les o
f F
resh
, P
eri
sh
ab
le,
Re
frig
era
ted
, F
oo
d P
ois
on
ing
Pro
du
cts
& S
em
i-p
rese
rve
d
Pro
du
cts
Fro
ze
n S
am
ple
s2
50
g
no
t e
xce
edin
g 3
0°C
Ste
rile
Pa
cka
gin
g/
Orig
ina
l P
acka
gin
g
PA
CK
AG
ING
MIN
IMU
MQ
UA
NT
ITY
NE
ED
ED
PA
RA
ME
TE
R M
IKR
OB
IOLO
GI
OR
GA
NIS
MA
PE
TU
NJU
K:
a)
To
tal
Pla
te C
ou
nt
b)
Co
lifo
rm
c)E
.co
li
d)
Ye
ast
& M
ou
ld C
ou
nt
OR
GA
NIS
MA
PA
TO
GE
NIK
:
a)
Sta
ph
ylo
cocc
us
au
reu
s
b)
Ba
cill
us
cere
us
c)Sa
lmo
ne
lla
sp
p
d)
E.c
oli
01
57
e)
Vib
rio
ch
ole
rae
f)V
ibri
o p
ara
ha
em
oly
�cu
s
g)
List
eri
a m
on
ocy
tog
en
es
h)
Ca
mp
ylo
ba
cte
r je
jun
i
44
jad
ua
l 1
.12 p
an
du
an
ru
juk
an
pa
nta
s u
nt
uk
uji
an
mik
ro
bio
lo
gi
B.cereus and
Bacillus spp.
Campylobacter
spp.
Esch. coli
Listeria
monocytogenes
Salmonella spp.
Staph. aureus
Vibrio spp.
//
//
/
*/
/*
//
//
//
//
/
/*
**
ch
ee
se
**
##
##
/
ice
-cre
am
#*
/#
##
milk
(liqu
id)
- u
ntr
ea
ted
#/
/*
##
pa
ste
urise
d#
/#
#
milk
-ba
se
d d
rin
ks -
pa
ste
uri
se
d/
##
milk
(dried)
//
/#
##
yo
gh
urt
*/
##
*/
/
//
//
//
sh
ell
/
po
wd
ere
d#
//
##
raw
fish
//
co
oke
dfish
/*
/*
//
/
pre
se
rve
d/
//
//
/*
*
fru
it ju
ice
**
**
*/
ca
rbo
na
ted
so
ft d
rin
ks
/*
**
*/
/*
**
**
/
red
, sa
usa
ge
s,
po
ultry
(ra
w)
**
**
/*
co
oke
d/
/*
//
//
*
cu
red
me
ats
**
*/
**
*
rea
dy-t
o-e
at
foo
ds
//
//
//
*
co
ok-c
hill
, co
ok-f
ree
ze
//
//
/
ha
nd
s/
//
foo
d s
urf
ace
s a
nd
equ
ip
me
nt
**
//
/
clo
ths
**
*
fre
sh
//
*/
*
bla
nch
ed
an
d f
roze
n/
/
po
tab
le#
#
na
tura
l m
ine
ral w
ate
r#
#
:
# = 'sta
tuto
ry' t
ests
/ = 'r
eco
mm
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