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DAFTAR ISI

HALAMAN JUDULiLEMBAR PERNYATAANiiLEMBAR PENGESAHAANiiiABSTRAKSivKATA PENGANTARviDAFTAR ISIviiDAFTAR TABELixDAFTAR GAMBARxDAFTAR LAMPIRANxi

BAB I PENDAHULUANLatar belakang1Rumusan Masalah2Batasan Masalah3Hipotesa3Tujuan Penelitian3Manfaat Penelitian4BAB II TINJAUAN PUSTAKA2.1. Metampiron52.1.1. Sifat Fisikokimia52.2. Piridoksin HCl62.2.1 Sifat Fisikokimia62.3. Tiamin HCl72.3.1. Sifat Fisikokimia72.4. Kromatografi Cair Kinerja Tinggi (KCKT)82.4.1. Parameter KCKT92.4.2. Komponen KCKT122.4.2.1. Wadah Fase Gerak122.4.2.2. Pompa132.4.2.3. Tempat Injeksi Sampel (Injektor)132.4.2.4. Kolom142.4.2.5. Detektor142.4.2.6. Perekam (Recorder)152.5. Validasi Metode Analisis152.5.1. Kecermatan (Accuracy)152.5.2. Keseksamaan/Ketelitian (Precision)162.5.3. Linearitas172.5.4. Batas Deteksi (Limit of Detection)182.5.5. Batas Kuantifikasi (Limit of Quantification)182.5.6. Spesitifitas18BAB III METODE PENELITIAN3.1. Waktu dan Tempat Penelitian203.2. Alat-alat203.3. Bahan-bahan203.4. Rancangan Penelitian203.4.1. Penyiapan Bahan203.4.1.1. Pembuatan Fase Gerak203.4.1.2. Pembuatan Larutan Baku Pembanding Metampiron213.4.1.3. Pembuatan Larutan Baku Pembanding Piridoksin HCl213.4.1.4. Pembuatan Larutan Baku Pembanding Tiamin HCl213.4.2. Penyiapan Alat223.4.3. Tahapan Penelitian223.4.3.1. Penentuan Komposisi Fase Gerak223.4.3.1. Uji Selektifitas223.4.3.1. Uji Kesesuaian Sistem233.4.3.1. Linearitas233.4.3.1. Akurasi243.4.3.1. Presisi253.4.3.1. Penentuan Batas Deteksi (LOD) dan Batas Kuantifikasi (LOQ)25BAB IV HASIL DAN PEMBAHASAN27BAB V KESIMPULAN DAN SARAN5.1. Kesimpulan405.2. Saran40DAFTAR PUSTAKA4LAMPIRAN4


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Table of Content

Table of Content

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